in this paper, shielding effectiveness (se) of a perforated enclosure with imperfectly conducting walls is evaluated. to this end, first, an accurate numerical technique based on method of moments (mom) ispresented. in this method, lossy metallic walls of the enclosure are replaced by equivalent electric surfacecurrent sources. then, the impedance boundary condition on the imperfectly conductin...

This paper concerns quality assurance of arsenic determination in urine using the graphite furnace AAS method after toluene extraction. Obtained analytical results are used for validation and quality assurance purposes. The investigated urine samples were acquired from the workers of a large coal-fired Slovak power plant. In the proposed analytical method the following metrological characterist...

Residue identification in a pharmaceutical manufacturing environment involves; the cleaner, primary ingredients, excipients, decomposition products, and preservatives. This document is intended to help with the cleaner residue identification. Residue detection method selection for cleaners can involve specific methods for specific cleaner ingredients such as; high performance liquid chromatogra...

Method validation presents a detailed investigation of analytical method and provision of the evidence that the method, when correctly applied, produces results that fit to the purpose. In order to achieve the method validation scope efficiently, experimental design presents a very useful tool. The greatest benefits of such approach could be seen in robustness testing through the provision of v...