acluster[ pt (reo )(?-dppm) ][reo ],2 [dppm=ph pch ] with oxidaton of [pt re(co) ](?-dppm) ][pf ] is prepred . crystals are triclinic,pl; a= 14.154(4)?, b=14.213(3) ?,c = 20.522(4) ? , a = 78.938(14)?, ?= 75.812(19) ? , ?= 74,957(22) ? ;v = 3828.9(1 5) ? ,z =2 ; eraf-noniu cad4 difhctorneter with mo- k radiation, ? = 0.71073 ? ; r = 0.069, r = 0.077 for 284 parameters and 5414 reflections with ...