in this research, kinetics of carbothermic reduction of molybdenite in the presence of different amounts of sodium carbonate has been studied. mixed powders consisting of molybdenite, graphite and sodium carbonate with three mole-ratios of 1:4:2,1:4:3 and 1:4:4 were mechanically activated for 40 hours. the results of x-ray diffraction on activated samples showed that no reaction occurrs in diff...

storage of hydrogen is one of the key challenges in developing hydrogen economy. magnesium hydride (mgh2) is an attractive candidate for solid-state hydrogen storage for on-board applications. in this study, 10 wt.% zrb2 was co-milled with magnesium hydride at different milling times to produce nanocrystalline composite powder. the effect of milling time and additive on the hydrogen desorption ...

The purpose of this study is preparation polyaniline–lead ferrite, polyaniline–cobalt ferrite and polyaniline/nickel thin layers. electromagnetic pollution a serious problem in the world that can be solved by interference (EMI) shielding. EMI layers synthesized conductive layer composed magnetic particles. Crystallite size samples was studied (XRD) analyze via Debye–Scherrer Williamson–Hall equ...

X-ray diffraction analysis is one of powerful tools on the dislocation and this method can be applied reasonably for many metals with isotropic crystal structure such as bcc fcc. In study, modified Williamson-Hall was martensitic steels containing 0.006 – 0.26 mass% carbon proved that value density increases increasing content. However, solute have bct characterized by different lattice constan...

We successfully synthesized Cu/Cu2O nanocomposites using the wet chemical synthesis method. All X-ray diffraction (XRD), Reference Intensity Ratio (RIR), and Rietveld refinement methods confirmed that compounds Cu Cu2O are free of impurities. Scanning Electron Microscope (SEM) Transmission electron microscopy (TEM) images show morphology interactions in structure. The formation mechanism is als...

The effect of CaO on the formation of β- and γ-zirconia nanoparticles from α-zirconia was investigated and their stability evaluated via mechanical activation. α-ZrO2+8.5wt%CaO powder was milled for 2-150 hours with ball-to-powder weight ratios (BPWR) of 40:1 and 60:1. Structural evaluations were conducted using X-Ray diffraction and scanning electron microscope (SEM). Thermal analysis wa...

The new triphasic potassium−substituted hydroxyapatite (KHAP), β−tricalcium phosphate (β−TCP), and calcium pyrophosphate (CPP) proportions using easy sol−gel method were synthesized. The prepared powders was characterized by X–ray diffraction (XRD), Fourier transform infrared (FTIR), Differential thermal behavior (DTA) analysis, Energy Dispersive X–ray Analysis (EDXA), and Brunauer–Emmett–Telle...