mcm-41 is one of the groups of mesoporous materials that have wide applications as adsorbents, ion exchangers and catalyst supports. in this work spherical and rod-like mcm-41s were synthesized in homogeneous and heterogeneous reaction media, respectively. for synthesis of these materials the cationic surfactant cetyltrimethylammonium bromide (ctmabr) was used as template and tetraethylorthosil...

in this paper we report synthesis of fe2tio5-5a zeolite (z5a) nanocomposites with 5%, 10% and 20% weight percent of fe2tio5 in 5a zeolite in stearic acid media after calcination of the gel samples obtained at 600-900°c for 2 hrs. the powder x-ray diffraction (xrd) patterns have been used for characterization of the prepared samples. the scanning electron microscopy (sem) images and x-ray energy...

in the present investigation, a novel adsorbent, ionic liquid modified magnetic nanoparticles (il-fe3o4), was successfully synthesized and characterized by ft-ir spectroscopy, thermogravimetric analysis (tga), xrd analysis, scanning electron microscopy (sem) and theory of brunauer, emmett, and teller (bet) for removal of reactive orange 122 (ro-122) from aqueous solutions. the effects of variou...

This study investigates the efficacy of a prepared Ni/θ-Al 2 O 3 catalyst during pyrolytic conversion Parachlorella kessleri HY-6 and compares results with non-catalytic conversion. The was characterized by techniques such as Brunauer–Emmett–Teller (BET) for surface area, acidity, X-ray powder diffraction (XRD). Isoconversional combined kinetic methods were used to kinetics process. at 10, 20, ...

Modifying of HY/Zeolite is by loading nickel for applying catalyst in thermal catalytic cracking furfural extract-40 from the lubricating base oil unit. The study involved characterizing HY-zeolite and promoted with X-ray diffraction analysis, Scanning electron microscopy (SEM), BET (Brunauer, Emmett, Teller), infrared ray analyses FTIR. tubular reactor a fixed bed two type catalysts; HY/zeolit...

The synthesis of orthoferrites the type La1−xCexFeO3+x/2, x = 0.00, 0.01, 0.03, 0.05, and 0.07, by applying a simple effective mechanochemical transformation from constituent oxides is presented. Physicochemical methods such as powder X-ray diffraction (XRD), transmission electron microscopy (TEM), UV–Vis spectroscopy, Brunauer–Emmett–Teller (BET) adsorption were applied to gain information abo...

BACKGROUND The inhalation of combustion-derived nanoparticles (CDNPs) is believed to cause an oxidative stress response, which in turn may lead to pulmonary or even systemic inflammation. OBJECTIVE AND METHODS In this study we assessed whether the in vivo inflammatory response--which is generally referred to as particle toxicity-of mice to CDNPs can be predicted in vitro by a cell-free ascorb...

sulfated titania nanoparticles (so42-/tio2 nps) were synthesized using titanium tetraisopropoxide (ttip) by the sol-gel method. the structure and morphology of the prepared nanocatalyst was characterized using x-ray diffraction (xrd), scanning electron microscopy (sem) and brunauer–emmett–teller (bet) methods as well as fourier transform infrared (ft-ir) and energy dispersive x-ray (edx) spectr...

in this work, the template, monomer and cross-linker with the ratio of 1:8:40 were used to synthesize molecularly imprinted polymers (mips) for extraction of the bioactive chemical compounds from some traditional herbs as a sorbent material. quercetin, methacrylic acid (maa), trimethylolpropanetrimethacrylate (trim) and tetrahydrofuran (thf) were used as a template, functional monomer, cross-li...

the fe-mcm-22 zeolite was found to be an efficient solid heterogeneous catalyst for synthesis of dihydropyrano [2,3-c] pyrazoles via one pot four component reaction of ethyl acetoacetate, hydrazine hydrate, aromatic aldehyde and malononitrile in aqueous alcohol. the catalyst was synthesized by hydrothermal method under autogenous pressure and modified by fe (iii) ion exchange. the prepared cata...