نتایج جستجو برای: synthesis dynamic light scattering dls
تعداد نتایج: 1270176 فیلتر نتایج به سال:
This study is focused on synthesis of nano-colloidal silica via alkaline water glass solution. Sodium ions of water glass were removed by cation exchanging in a resin column to obtain the silicic acid which was titrated to the solution of sodium silicate. Concentration of the colloidal silica and pH value of the solutions were controlled using different concentrations of alkaline sodium silicat...
Core-shell microgels made of the thermoresponsive polymer poly(N-isopropylacrylamide) (PNIPAM) and silica nanoparticles as inorganic cores were investigated by dynamic light scattering (DLS) and small angle neutron scattering (SANS). In order to study the response of the particles upon changes of temperature, experiments were done in a temperature interval close to the volume phase transition t...
The aqueous extract of Ocimum basilicum leaves and zinc salts (zinc sulphate) was used as precursors in this investigation to create oxide nanoparticles. ultraviolet-visible spectroscopy, scanning electron microscopy, Dynamic light scattering (DLS) were characterize the produced (SEM), Energy-dispersive X-ray analysis (EDX), Because UV-Vis spectra exhibit absorption peaks 350 nm range. DLS prov...
In the present paper we describe a phase transfer of aqueous synthesized gold nanoparticles (AuNPs) from water to toluene using secondary amines: dioctylamine, didodecylamine, and dioctadecylamine. The effect of the hydrocarbon chain length and amount of amines on the transfer efficiency were investigated in the case of nanoparticles (NPs) with three different sizes: 5, 9, and 13 nm. Aqueous co...
The impact of biocompatible additives on the fibrillation and defibrillation of proteins provides valuable insight into the development of suitable formulations for the treatment of protein-related diseases or the storage of proteins in the laboratory. We have studied the effects of the addition of sodium deoxycholate (NaDC) and sodium salicylate (NaSal) on the fibrillation of bovine serum albu...
An adsorbed layer of a cationic polyelectrolyte, poly(diallyldimethyl-ammonium) chloride (PDADMAC) on negatively charged colloidal latex particles was investigated by small-angle neutron scattering (SANS) and dynamic light scattering (DLS). SANS gives a layer thickness of 8 +/- 1 A and a polymer volume fraction of 0.31 +/- 0.05 within the film. DLS gives a somewhat larger thickness of 18 +/- 2 ...
The effect of polyoxyethylene type nonionic surfactants (C12En n=3, 4, 5, 6, 7 and 8) on the aqueous solution of sodium dodecyl sulfate (SDS) in absence and presence of NaCl was examined using small-angle neutron scattering (SANS), dynamic light scattering (DLS), and viscosity measurements. Upon addition of C12En, micellar size of SDS was found to increase significantly, and such micellar elong...
Enzyme/polymer/gold nanoparticle hybrids, called "nanozymes", were prepared and structurally analyzed by dynamic light scattering (DLS), ultraviolet-visible spectroscopy, and zeta-potential and transmission electron microscopy (TEM) measurements, which showed that the nanozyme particles were mainly composed of a single gold nanoparticle, on whose surface the enzyme and polymer were coimmobilize...
Ferromagnetic iron oxide nanoparticles of about 33nm in diameter were synthesized by hightemperature decomposition of an iron–oleate complex, using octadecene as the solvent. These particles were subsequently coated with polyN-isopropylacrylamide (pNIPAAm) by a surfactant exchange method. Temperature-sensitive behavior of these particles was studied using ac susceptibility and dynamic light sca...
Biological production of silver nanoparticles, due to its high antimicrobial properties and environmental compatibility, can be used as an alternative to antibiotics. The aim of this study was to optimize the green synthesis of silver nanoparticles using fruit extract of Bunium persicum Boiss and investigate the antimicrobial effect of nanoparticles against Escherichia coli and Staphylococcus a...
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