A synthesis of [“Qcopolamine capable of clinical delivery of this agent in high specific activity is described. The precursor [“Clformaldehyde was produced by catalytic oxidation of [“C]CH,OH over metallic silver and was used to N-“C-methylate norscopolamine using aqueous neutral potassium phosphite as the reducing agent. The labeling reaction was complete after 5min at 7580°C and the [“Clscopo...

Nanoparticles have the advantage of a superior surface area to volume ratio, and thus such materials are useful for enzyme immobilization. A silver nanoparticle coated cotton fabric (AgNp-CF) is used immobilize camel liver catalase in present work. The effect loading levels AgNp inside fabrics on immobilization was investigated. results revealed that 6 mL level precursor (silver nitrate, 2 mM) ...

as a new precursor, [tris(2-hydroxyacetophenato) triaqua(iii)], [y(hap)3(h2o)3]; complex was used in thermal decomposition process for the synthesis of rod-like high-temperature ceramic ybco with length of about 320-350 nm and diameters 60–90 nm. the as-synthesized products were characterized by xrd, ft-ir, tem, sem and edx analyses. the results showed that by using fine raw materials, the calc...

This study presents the use of modified coffee husk and lignin as sorbents in heavy metal ions sorption Pb(II), Cd(II), Cr(III), Cu(II) an aqueous solution. The modification was carried out by impregnation method, using silver nitrate (AgNO3) sodium borohydride (NaBH4) a nanoparticles’ (NPs) precursor, reducing agent, respectively. obtained nanocomposite material morphologically characterized e...

This work focuses on the preparation of silver nanoparticles (AgNPs) by a green synthesis using seed extract Derris trifoliata. The optimum time and temperature for extraction seeds were determined FTIR analysis. acted as reducing agent nitrate was used metal precursor AgNPs. Optimization reaction conditions AgNPs its characterization done UV-Vis spectroscopy, FTIR, HRTEM SAED images. UV- Visib...

BACKGROUND Green approach in synthesizing metal nanoparticles has gain new interest from the researchers as metal nanoparticles were widely applied in medical equipment and household products. The use of plants in the synthesis of nanoparticles emerges as a cost effective and eco-friendly approach. A green synthetic route for the production of stable silver nanoparticles (Ag-NPs) by using aqueo...

A cluster obtained in high yield from the reduction of a silver-thiolate precursor, Ag-SCH(2)CH(2)Ph, exhibited a single sharp peak near 25 kDa in the matrix-assisted laser desorption mass spectrum (MALDI MS) and a well-defined metal core of ~2 nm measured with transmission electron microscopy (TEM). The cluster yields a single fraction in high-performance liquid chromatography (HPLC). Increase...

Silver nanoparticles (Ag-NPs) were synthesized into the interlamellar space of montmorillonite (MMT) by using the γ-irradiation technique in the absence of any reducing agent or heat treatment. Silver nitrate and γ-irradiation were used as the silver precursor and physical reducing agent in MMT as a solid support. The MMT was suspended in the aqueous AgNO(3) solution, and after the absorption o...

This paper presents the results of studying process laser formation microstructures from silver nanoparticles in nanoporous quartz glasses. Glass samples were impregnated with organometallic molecules Ag(hfac)COD a supercritical carbon dioxide environment. The point and linear was carried out by high-frequency (70 MHz) femtosecond radiation wavelength 525 nm energy pulse up to 1 nJ. It found th...

in this paper, we report on the synthesis of cu nanoparticles through a single-precursor route by controlling the growth temperature. selective adsorption of oleylamine on various crystal planes may play an important role in the growth process. the understanding of this self-assembling process will help us develop reliable and reproducible methods to synthesis other three dimensional nanostruct...