نتایج جستجو برای: salt assisted liquid liquid extraction

تعداد نتایج: 568103  

2013
Xiao-Hua Xiao Zhi-Quan Yuan Gong-Ke Li

A rapid method of microwave-assisted extraction coupled with high-speed counter current chromatography and UV detector was established for the preparation of phytosterols from edible marine algae. Extraction conditions, namely microwave power, liquid/solid ratio, irradiation time and extraction temperature were optimized using orthogonal array design. The microwave-assisted extraction of Undari...

2017
Yang Sun Song Ding He Huang Yi Hu

Background: In recent years, ionic liquids and enzymes have been widely used in the separation and extraction processes of natural products. Chlorogenic acid (CGA) has important biological and pharmacological activities. It is significant to develop a green and efficient method to extract GCA from Flos Lonicera japonica (FLJ) by integrating the advantages of the ionic liquids and enzymes. Resul...

Journal: :Journal of agricultural and food chemistry 2013
Shekhar U Kadam Brijesh K Tiwari Colm P O'Donnell

Marine algae are a rich source of bioactive compounds. This paper outlines the main bioactive compounds in marine algae and recent advances in novel technologies for extracting them. Novel extraction technologies reviewed include enzyme-assisted extraction, microwave-assisted extraction, ultrasound-assisted extraction, supercritical fluid extraction, and pressurized liquid extraction. These tec...

Journal: :iranian journal of pharmaceutical research 0
m amini m khanavi a shafiee

a rapid, simple and sensitive high-performance liquid chromatography method was developed for determination of ciprofloxacin in plasma by means of ultraviolet detection. ofloxacin was used as an internal standard and separation carried on a novapak c18 column using a mobile phase of 0.01 m phosphate buffer (ph =2.6): methanol (82: 18 v/v). extraction of drug was performed from plasma by liquid-...

A simple, fast and effective pre-concentration method for the determination of Cu (copper) and Ni (nickel) was developed using a Surfactant Assisted Dispersive Liquid-Liquid Microextraction (SA-DLLME) coupled by UV-Vis spectrophotometry in marine brown algae. The complexing agent was 1- (2- pyridylazo) – 2 - naphthol (PAN).The effects of various experimental parameters in the extraction ste...

In this work, two approaches based on Dispersive Liquid-Liquid MicroExtraction (DLLME) and Dispersive Liquid-Liquid MicroExtraction based on Solidification of Floating Organic Drop (DLLME-SFO) were compared for the extraction and preconcentration of crocin from saffron and biological samples. Different DLLME and DLLME-SFO parameters influencing the extraction efficiency were studied and opt...

Journal: :Electrophoresis 2012
Caihong Zhou Shanshan Tong Yunxia Chang Qiong Jia Weihong Zhou

Ionic liquid (IL) based dispersive liquid-liquid microextraction (DLLME) with back-extraction coupled with capillary electrophoresis ultraviolet detection was developed to determine four phenolic compounds (bisphenol-A, β-naphthol, α-naphthol, 2, 4-dichlorophenol) in aqueous cosmetics. The developed method was used to preconcentrate and clean up the four phenolic compounds including two steps. ...

Journal: :Talanta 2015
Elena Fernández Lorena Vidal Daniel Martín-Yerga María del Carmen Blanco Antonio Canals Agustín Costa-García

A novel approach is presented, whereby gold nanostructured screen-printed carbon electrodes (SPCnAuEs) are combined with in-situ ionic liquid formation dispersive liquid-liquid microextraction (in-situ IL-DLLME) and microvolume back-extraction for the determination of mercury in water samples. In-situ IL-DLLME is based on a simple metathesis reaction between a water-miscible IL and a salt to fo...

2016
A. Daneshfar T. Khezeli

A very simple, rapid and sensitive dispersive liquid-liquid microextraction (DLLME) followed by gas chromatography and flame ionization detection (GC-FID) was developed for the determination of phenol and carvacrol in honey samples. A mixture of 100 μl dichloromethane (extraction solvent) and 0.5 ml acetonitrile (disperser solvent) was rapidly injected into sample solution. Thereby a cloudy sol...

Journal: :Journal of Chemistry 2021

Isolation and enrichment of multiclass pesticides’ residue, namely, fungicides (benalaxyl), herbicides (atrazine), carbamate insecticides (carbofuran), organophosphate (chlorpyrifos), organochlorine (4,4′-DDT), pyrethroid (bifenthrin), were made by combining acetone-based salting-out assisted extraction with the dispersive liquid-liquid microextraction (SADLLME) method, followed high-performanc...

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