the perovskite-type oxides strontium-substituted lanthanum nickelate (lsno) were prepared by a coprecipitation method in the present of octanoic acid as surfactant. the phase composition, morphology,lattice parameters and size of nanoparticles in these materials were characterized through fourier transform infrared spectroscopy (ft-ir), x-ray diffraction (xrd), scanning electron microscopy (sem...

zro2 nanopowder was prepared by the sol-gel auto-combustion method. the product was characterized by x-ray diffraction (xrd), energy dispersive analysis of x-ray (edx) and scanning electron microscopy (sem). the average crystalline size of zro2 was obtained 62 nm. also, photocatalytic removal of nitrophenol from aqueous solution by using nanoscale zro2 under uv light irradiation was studied. th...

cobalt (ii) chloride was used as a precursor to prepare co 3 o 4 nanotubes in reverse micelles. tween 80 was added as surfactant. the products were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem) and transmission electron microscopy. the diameter of co 3 o 4 nanotubes was about 58 nm and the average length of them was around 261 nm. the study provides a simple and e...

sn02 nanowires with diameters of 30 — 200 nm have been synthesized by using carbothermalprocess via a thick film of tin dioxide and carbon powder precursor. the nanowires werecharacterized by x-ray power diffraction (xrd), scanning electron microscopy (sem),transmission electron microscopy (tem) and selected area electron diffraction (saed).the gas sensing characteristic of nanowires toward eth...

cobalt oxide (co3o4) nanoparticleshave been synthesized by hydrothermal method using mixture of cobalt(ii)chloride, triton x-100 and koh in an autoclave at 180 °c for 6 h followed by heating at 400 ºc for 3 h in air. the product have been characterized by fourier transform infrared (ft-ir), uv-vis spectroscopy, powder x-ray diffraction (xrd), scanning electron microscopy (sem) and transmission ...

cupric oxide nanostructures were synthesized via a simple reaction between copper nitrate and sodium hydroxide using a sonochemical-assisted method. the synthesized cuo was then characterized using x-ray diffraction, scanning electron microscopy, transmission electron microscopy, fourier transform infrared, ultraviolet-visible and photoluminescence spectroscopy. our studies show that the cuo na...

bismuth sulfide nano-rods and nano-flowers were synthesized via a hydrothermal reaction at a relatively low temperature. thioglycolic acid is used as sulfur source and capping agent simultaneously. bi2s3 nanostructures were then added to acrylonitrile-butadiene-styrene (abs) copolymer. the thermal stability behavior of abs filled with bismuth sulfide nano-rods were investigated by thermogravime...

copper sulfate was used as a precursor to prepare cuo nanoparticles in reverse micelles (o/w microemulsion).  this is a technique which allows the preparation of ultrafine metal oxide nanoparticles within the size ranging from 50 to 60 nm. the preparation of nano copper (ii) oxide studied was investigated in the inverse microemulsion system. therefore the nucleation of metal particles proceeds ...

we evaluated the effect of fe/alumina catalyst contained different cadmium contents and two synthesis temperatures on producing carbon nanotubes by chemical vapor deposition of methane as a feedstock.  x-ray powder diffraction (xrd), n2 adsorption-desorption, scanning electron microscopy (sem), transmission electron microscopy (tem), raman spectroscopy and thermogravimetry analysis (tga) were u...

The Soft X-ray Undulator beamline at the NSLS supports a soft x-ray imaging program including scanning transmission microscopy, scanning photoemission microscopy, Gabor and Fourier transform holography, and large angle diffraction. Zone plates from an LBL Center for X-ray Optics/IBM collaboration are used as optical elements. The current instrumentation of the beamline and the experimental stat...