نتایج جستجو برای: pot condensation
تعداد نتایج: 46127 فیلتر نتایج به سال:
In this paper, we introduce Brønsted acidic ionic liquid (BAIL), (4-sulfobutyl) tris (4-sulfophenyl) phosphonium hydrogen sulfate as a green and efficient catalyst for the synthesis of 2,3-disubstituted quinoxaline derivatives via the one-pot condensation reaction of various o-phenylenediamine with 1,2-diketone derivatives. At all experiments, the desired products were synthesized successfully....
Acridinediones were synthesized by the one-pot Hantzsch condensation of an aromatic aldehyde, 5,5-dimethyl-1,3-cyclohexanedione, and aniline/4-methylaniline in refluxing water. This method has then been extended to the four-component reaction of an aromatic aldehyde, 5,5-dimethyl-1,3-cyclohexanedione, ethyl acetoacetate and ammonium acetate for the synthesis of polyhydroquinoline derivatives. Th...
in this thesis, we exploit a simple and suitable method for immobilization of copper(ii) complex of 4?-phenyl-terpyridine on activated multi-walled carbon nanotubes [amwcnts-o-cu(ii)-phtpy]. this nanostructure was characterized by various physico-chemical techniques. to ensure the efficiency and fidelity of copper species, the implementation of three-component strategies in click-chemistry all...
BACKGROUND The impact of global warming and associated climate changes have built up pressure to focus on the option of green chemistry over traditional one for long term sustainability of the environment. Considering the fact, for the first time, efficient HLE catalysed expeditious one-pot synthesis of highly functionalised 4-thiazolidinones has been developed. RESULTS These hybrid molecules...
this paper describes the applicability of 1,3-dichloro-5,5-dimethylhydantoin, as a cheap, stable and commercially available catalyst, in the promotion of the synthesis of 1,8-dioxo-octahydro-xanthenes (doxos) via the one-pot condensation of aldehydes and cyclic 1,3-dicarbonyl compounds. this novel synthetic method has the advantages of high yields, short reaction times, low cost and availabilit...
1, 4-Diazabicyclo [2.2.2] octane (DABCO) was employed as a catalyst for one-pot synthesis of pyrano[2,3-d] pyrimidinone derivatives and MWNT- pyrimidinones from condensation reactions of aromatic aldehydes, malononitrile and thiobarbituric acid and MWNT-COCl . This method delivers the advantages of a simple method, environment friendly procedure, mild reaction conditions and high returns. The m...
A simple and efficient protocol for the synthesis of N-substituted pyrroles from one-pot condensation reaction of 2, 5-dimethoxytetrahydrofuran with aryl/alkyl, sulfonyl and acyl amines in the presence of ZrOCl2•8H2O in water has been developed. This new method has the advantages of simple experimental and work-up procedure, high to excellent yields, easy availability, economical, eco-frien...
3,5-Bis(trifluoromethyl) phenyl ammonium triflate(BFPAT) catalyzed one-pot synthesis of indeno[1,2-b]pyridine compound derivatives by four-component condensation aldehyde, aromatic ketones, 1,3-indanedione, and acetate in ethanol. Accessible starting materials, Simplicity operation, green practical catalyst, easy purification, excellent yields are the key benefits current technique.
this research proposes an efficient and easy procedure for the preparation of amides or nitriles from aldehydes. such materials were prepared via one-pot three component condensation reaction of various aldehydes in the presence of nano-ticl4.sio2 as a catalyst under thermal conditions. all reactions proceeded in high yields and in a moderately short reaction time. meanwhile, oximes were obtain...
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