Ceria (CeO2) is an important rare earth oxide and has been widely investigated in the automotive exhaust puri cation, oxygen storage and release catalysis, and solid oxide fuel cell applications. In recent years, due to the excellent physical and chemical properties of nanosized particles, which are signi cantly different from those of bulk particles, there is considerable interest in enhancing...

A cordierite powder was synthesized from a batch composition of talc, diatomite and alumina. Sintered samples of the synthesized cordierite were characterized by X-ray diffraction (XRD), differential thermal analysis (DTA), and Rietveld analysis. The XRD analysis showed hexagonal or a-cordierite (indialite) as a major phase along with MgAl2O4 spinel and cristobalite as secondary phases in the s...

A zeolite NaA (LTA) membrane supported by an alumina porous support tube was characterized by Fourier Transform Infrared Attenuated Total Reflectance method (FTIR-ATR) with a diamond prism as the waveguide. A method using the FTIR-ATR was developed to estimate rapidly the EtOH/H2O pervaporation (PV) performance of the membrane. The Si-O asymmetric stretching vibration region of LTA membrane spe...

The electric, electronic, mechanical and thermal characteristics of high density electronic devices can be affected by the physico-chemical characteristics of base materials as well as by trace impurities. It is well known that soft errors caused by trace -emitting impurities are one cause of the faulty operation of electronic devices. This phenomenon was initially reported in May[1] in the 197...

Three different alumina sources (boehmite, aluminium nitrate and α-alumina particles) 12Ce-TZP powder containing 1 wt% lanthanum oxide were used to prepare 12Ce-TZP-based alumina-toughened-zirconia (ATZ) composites. The obtained ATZs had similar density phase composition, whereas the microstructures significantly different. Alumina-particle addition gave rise a typical ATZ microstructure consis...

Mechanical alloying (MA) is a solid-state powder processing technique involving repeated cold welding and fracturing of powder particles in a high-energy ball mill. It has been used to obtain nanocrystalline binary system FeNi. Fe and Ni elemental powders have been ball milled in a planetary mill (Pulverisette5, Fritsch) for various times up to several hours. The morphology of the powders was e...

The effects of sintering profiles on the densification behaviour of synthesized nanocrystalline hydroxyapatite (HA) powder were investigated in terms of phase stability and mechanical properties. A wet chemical precipitation method was successfully employed to synthesize a high purity and single phase HA powder. Green HA compacts were prepared and subjected to sintering in air atmosphere over a...

The evolution of size and size distribution during hydrothermal synthesis of nanocrystalline CoFe2O4 has been studied by in situ synchrotron powder X-ray diffraction (PXRD). Varying synthesis temperature or [OH(-)] concentration in the precursor proves to have no significant effect on the final volume-weighted nanocrystallite sizes (∼12 nm) of CoFe2O4. However, analysis by whole powder pattern ...

Novel uniform single-crystal boehmite leaf-like nanosheets with high anisotropy (with a lateral size of (4.5±0.5 μm)×(9.0±1.0 μm) and a thickness of 60–90 nm) and flower-like superstructures consisting of single-crystal petals were synthesized for the first time by a simple hydrothermal method. After calcination, those boehmite structures can be transformed into single-crystal gamma-alumina nan...