a solid phase extraction sorbent based on polyaniline/graphene nanocomposite is presented. the structure and morphology of synthesized nanocomposite were investigated by fourier transform infrared spectroscopy, field emission scanning electron microscopy, x-ray diffraction and thermal gravimetric analysis. the dispersive solid phase extraction was employed to the isolation and preconcentration ...

an air–assisted liquid–liquid microextraction method for the extraction and preconcentration of trace amounts of some synthetic phenolic antioxidants in biological fluids followed by their determination by gas chromatography–flame ionization detection has been reported. in this method the target analytes are extracted into a few microliters of carbon tetrachloride (extraction solvent) from an a...

A new carboxylic acid extractant, named 2-(dibutylcarbamoyl)benzoic acid, is prepared and its potential for selective solvent extraction and recovery of lead ions from industrial samples was investigated. The slope analysis indicated that the lead ions are extracted by formation of 1:2 metal to ligand complexes. The effect of the parameters influencing the extraction efficiency including kind o...

In this research mass transfer coefficient under jetting regime in different directions (from dispersed to continuous and continuous to dispersed phase) has been studied using an experimental setup. n-Butanol-succinic acid-water with low interfacial tension has been selected as experimental chemical system. The effects of various parameters such as jet velocity, nozzle diameter and the heig...

The solvent extraction of gallium from a concentrated Jajarm Bayer process liquor containing 164.90 g/l of Na2O, 86.70 g/l of Al2O3 and 106.02 ppm of gallium was investigated using 10 vol.% Kelex100, a 7-alkyl substituted-8 hydroxyquinoline as an extractant, 10 vol.% etanol as a modifier and kerosene as a diluent. At (Vo :Va = 1.0:1.0) ...

Polygalacturonase is one of the important enzymes used in various industries such as food, detergent, pharmaceutical, textile, pulp and paper. A novel liquid/liquid extraction process composed of surfactant and acetonitrile was employed for the first time to purify polygalacturonase from Durio zibethinus. The influences of different parameters such as type and concentration of surfactants, conc...

With a microfluidic droplet-based liquid/liquid extraction setup, we demonstrate that the extraction of an ionic analyte from complex matrices can be modulated by the interfacial Galvani potential difference and the extraction equilibrium follows the classical Nernst equation.

Thallium is widely found in nature, but the only inorganic stones full of this element are crookesite and lorandit. It isalso found in pyrites of copper, lead and inorganic stones. The element and its compositions are toxic and harmful to theenvironment; therefore, its application requires caution and further research. It is important to develop sensitive andaccurate analytical methods to deter...