نتایج جستجو برای: heating up solution synthesis

تعداد نتایج: 1769533  

In this study, the effect off adding SiO2 nanoparticles on the viscosity of base fluid is investigated experimentally. Base fluids are chosen among common heat transfer fluids such as ethylene glycol, transformer oil and water. In addition different volume percentages of ethylene glycol in water are used as ethylene glycol-water solution. In every base fluid different volume fractions of SiO2 n...

Karimzadeh, F., Ashrafi, A. , Ghaderi, S. ,

In the present study, the effect of time and base metal microstructure on the Transient Liquid Phase (TLP) bonding of 304L stainless steel was studied. TLP was performed at 1050 0C for 5 and 60 minutes on the coarse grain austenitic and martensitic microstructure using BNi-2 interlayer. To prepare martensitic microstructure, as-received 304L was rolled at -15 0C up to 80% rolling reduction. TEM...

2016
Hailong Dong Ana Kuzmanoski Tobias Wehner Klaus Müller-Buschbaum Claus Feldmann

Eu3+-modified carbon dots (C-dots), 3-5 nm in diameter, were prepared, functionalized, and stabilized via a one-pot polyol synthesis. The role of Eu2+/Eu3+, the influence of O₂ (oxidation) and H₂O (hydrolysis), as well as the impact of the heating procedure (conventional resistance heating and microwave (MW) heating) were explored. With the reducing conditions of the polyol at the elevated temp...

2003
S. Ravichandran

Microwave radiation, an electromagnetic radiation, is widely use as a source of heating in organic synthesis. The basic mechanisms observed in microwave assisted synthesis are dipolar polarization and conduction. Microwave assisted organic synthesis (MAOS) has emerged as a new “lead” in organic synthesis. The technique offers simple, clean, fast, efficient, and economic for the synthesis of a l...

Red pine leafs were applied for the green method preparation of MgO nano-plates. The MgO nano-plates were used for the one-pot synthesis of dihydropyrano [3,2-c] chromene derivatives. This procedure is very simple and affords excellent yields. MgO nanoplates were synthesized via a simple precipitation method with the using of an extract solution of red pine leaves. The XRD pattern shows a cubic...

Journal: :Molecules 2011
Hortensia Rodríguez Osnieski Martin Margarita Suarez Nazario Martín Fernando Albericio

Here we describe the efficient synthesis of alkyl 4-arylsubstituted-6-chloro-5-formyl-2-methyl-1,4-dihydropyridine-3-carboxylates and 4-arylsubstituted-4,7-dihydro-furo[3,4-b]pyridine-2,5(1H,3H)-diones via microwave-accelerated reaction of alkyl 4-arylsubstituted-2-methyl-6-oxo-1,4,5,6-tetrahydro-3-pyridinecarboxylates with the appropriate reagents. This eco-friendly approach to these valuable ...

Journal: :Chemistry 2007
Sung Hwa Jhung Taihuan Jin Young Kyu Hwang Jong-San Chang

Microporous materials, such as silicalite-1 and VSB-5 molecular sieves, have been synthesized by both microwave irradiation (MW) and conventional electric heating (CE). The accelerated syntheses by microwave irradiation can be quantitatively investigated by various heating modes conducted in two steps such as MW-MW, MW-CE, CE-MW, and CE-CE (in the order of nucleation-crystal growth). In the cas...

E. Salahi S. A. Tayebi fard S. M. M. Shafiei

In this study the synthesis of molybdenum oxide nano-whiskers with circular cross-section is performed. In some areas, it was observed that also some whiskers have open tips exhibiting their hollow structures. These whiskers have side dimensions ranging 2-5 μm with an average diameter in the nanometer rang. The structure suggested the vapor-liquid-solid growth mechanism (VLS). Scanning elect...

1998
U. Hechtfischer Z. Amitay P. Forck M. Lange J. Linkemann M. Schmitt U. Schramm D. Schwalm R. Wester D. Zajfman A. Wolf

U. Hechtfischer,1 Z. Amitay,2 P. Forck,1 M. Lange,1 J. Linkemann,1 M. Schmitt,1 U. Schramm,1 D. Schwalm,1 R. Wester,1 D. Zajfman,2 and A. Wolf1 1Max-Planck-Institut für Kernphysik und Physikalisches Institut der Universität Heidelberg, 69029 Heidelberg, Germany 2Department of Particle Physics, Weizmann Institute of Science, Rehovot, 76100, Israel (Received 12 November 1997) Photodissociation of...

S. A. Hosseini, S. Noori

In the present work, an engineering method is developed to predict laminar and turbulent heating-rate solutions for blunt reentry spacecraft at hypersonic conditions. The calculation of aerodynamic heating around blunt bodies requires alternative solution of inviscid flow field around the hypersonic bodies. In this paper, the procedure is of an inverse nature, that is, a shock wave is assumed a...

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