Plastic deformations, such as those obtained by shot peening on specimen surface, are an efficient way to improve the mechanical behavior of metals. Generally, scanning electron microscopy (SEM) and electron backscattered diffraction (EBSD) are commonly used to observe the complex microstructural evolutions, such as grain refinement and phase transformation, induced by the surface treatment. In...

the permeability and the power losses are very important properties of non-oriented electrical sheets. the existence of a crystallographic easy magnetization plane and direction makes the distribution of grain orientations (texture) the most important factor in the improvement of the quality of a soft magnetic material [1]. the optimum texture is a fibre texture in which all the grains have a <...

The crystallization behavior of a glass with the composition 54.7 SiO2·10.9 Al2O3·15.0 MgO·3.4 ZrO2·16.0 Y2O3 is studied using X-ray diffraction (XRD), scanning electron microscopy (SEM) including electron backscatter diffraction (EBSD) and (scanning) transmission electron microscopy [(S)TEM] including energy-dispersive X-ray spectrometry (EDXS). This glass shows the sole surface crystallizatio...

The electron backscatter diffraction (EBSD) characterization of irradiated Al-B shows that there is a high concentration defect region around the borides. Nanoscale speckle particles were successfully prepared on surface before and after irradiation, then mesoscale strain during in-situ deformation was obtained by digital image correlation (DIC) technique. results slip band bypass such an area ...

This study presents a comprehensive evaluation of the effects multi-channel spiral twist extrusion (MCSTE) processing on mechanical properties and structural evolution AA5083. The texture developed were mapped by electron backscatter diffraction (EBSD) for three successive passes compared with an as-annealed plate. An hardness tensile was presented correlated EBSD findings. displayed results re...

The microstructure resulting from plastic deformation of metals typically contains heterogeneity on several length scales. This is also true for samples deformed to large strains, where an important form of heterogeneity is in the variation in microstructural refinement by high angle boundaries. A methodology for quantifying this type of heterogeneity based on the identification of areas classi...

Electron backscatter diffraction (EBSD) has been used to examine the plastic deformation of an ex-service 316 austenitic stainless steel at 297K and 823K at strain rates 3.5x10 -3 s -1 – 4x10 -7 s -1 . The distribution of local misorientations was found to depend on the imposed plastic strain following a lognormal distribution at true strains < 0.1 and a gamma distribution at strains > 0.1. At ...

Grain boundary migration is an important mechanism of microstructural modification both in rocks and in metals. Combining detailed cathodoluminescence (CL) and electron backscatter diffraction (EBSD) analysis offers the opportunity to relate directly changes in crystallographic orientation to migrating boundaries. We observe the following features in naturally heated quartz grains from the ther...

In this study we present microstructural data from hydrothermal veins in the sedimentary cover and the igneous basement recovered from Hole U1414A, Integrated Ocean Drilling Program (IODP) Expedition 344 (Costa Rica Seismogenesis Project), to constrain deformation mechanism operating in the subducting Cocos Plate. Cathodoluminescence studies, mechanical e-twin piezometry and electron backscatte...