Abstract: Nanoscale FeS2 was synthesized via a simple hydrothermal method and was decorated by hydrothermal carbonization (FeS2@C). The structural properties of the synthesized materials detected by X-ray diffraction (XRD), together with the morphologies characterized by scanning electron microscopy (SEM) and transmission electron microscopy (TEM) indicated that the hydrothermal carbonization o...

The corrosion behavior of pure Fe under a Na₂SO₄ deposit in an atmosphere of O₂ + H₂O was investigated at 500 °C by thermo gravimetric, and electrochemical measurements, viz. potentiodynamic polarization, electrochemical impedance spectroscopy (EIS), and surface characterization methods viz. X-ray diffraction (XRD), and scanning electron microscope (SEM)/energy dispersive spectroscopy(EDS). The...

A graphite powder disk sandwiched between two nickel screens was used as a lithium-insertion working electrode. Electrochemical impedance spectroscopy (EIS), galvanostatic intermittent titration (GIT) using pulsed microcurrent, and in-situ intrinsic resistance measurements were used for the evaluation of kinetics and intrinsic (i.e. physical) resistance changes during charge–discharge cycling f...

polymer-clay nanocomposite coatings have attracted much attention because of impressive enhancements of coating properties. in this research, both commercially available and isophoronediamine-modified montmorillonite clays were used to obtain epoxy-clay nanocomposite coatings. these nanocomposite materials with different clay loadings in the form of coatings were applied to cold-rolled steel (c...

The biodegradable inhibitors, which could effectively reduce the rate of corrosion of carbon steel, were investigated by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). The mixed-type inhibitors extracted from Eriobotrya japonica Thunb. leaf exhibited excellent inhibition performance, and the inhibition efficiency for carbon steel reached 90.0% at 298 K in hydroch...

Here, we proposed to test the limits of bounded diffusion impedance model by using electrochemical spectroscopy (EIS) measurements in a microfluidic device architecture bearing set microelectrodes integrated microchannel. This EIS Nyquist plot behaviour was currently modelled with Randles equivalent circuit. In this work, one main advantages for PyEIS (a Python-based Electrochemical Impedance S...

A novel biochemical sensor was assembled on a glass carbon electrode by a electrodeposition process. Gold nanoparticles were deposited by potential +1.5 V on the glass carbon electrode. CT-DNA was deposited by potential +1.5 V on the gold nanoparticles array electrode. The properties of the modified electrode were characterized by electrochemical impedance spectroscopy (EIS), X-ray photoelectro...

Polypyrrole (PPy) films of different thickness were characterized by electrochemical impedance spectroscopy (EIS) measurements in acetonitrile and aqueous solutions, containing 0.1 M NaClO4 or sodium dodecylsulfate as the dopant. The PPy films were electrochemically deposited on Pt, and their electrochemical properties studied by cyclic voltammetry. Impedance spectra were obtained at potentials...

J. Przondziono, Faculty of Materials Science and Metallurgy, Silesian University of Technology, Katowice, Poland, W. Walke, Faculty of Biomedical Engineering, Silesian University of Technology, Zabrze, Poland Quality of applied guide wires conditions the course of treatment and its success to a great extent. In order to simulate conditions that can be found in blood vascular system samples were...

the synthesis of polyaniline- fe2o3 nanocomposite coating on aluminum alloy 5052 (aa5052) surface has been investigated by using the galvanostatic method. the anticorrosion performance of polyaniline-fe2o3 coating was investigated in 3.5% nacl solution by the open- circuit potential (ocp), tafel polarization technique and electrochemical impedance spectroscopy (eis). the corrosion rate of polya...