In this work, a two-step electrodeposition strategy is developed for the synthesis of core-shell Co₃O₄@CoS nanosheet arrays on carbon cloth (CC) for supercapacitor applications. Porous Co₃O₄ nanosheet arrays are first directly grown on CC by electrodeposition, followed by the coating of a thin layer of CoS on the surface of Co₃O₄ nanosheets via the secondary electrodeposition. The morphology co...

Transient local pH changes in the brain are important markers of neural activity that can be used to follow metabolic processes that underlie the biological basis of behavior, learning and memory. There are few methods that can measure pH fluctuations with sufficient time resolution in freely moving animals. Previously, fast-scan cyclic voltammetry at carbon-fiber microelectrodes was used for t...

Poly(methylene blue) and electrochemically reduced graphene oxide composite film modified electrode (PMB-ERGO/GCE) was successfully fabricated by electropolymerization and was used for simultaneous determination of uric acid (UA) and xanthine (Xa). Based on the excellent electrocatalytic activity of PMB-ERGO/GCE, the electrochemical behaviors of UA and Xa were studied by cyclic voltammetry (CV)...

Textile wastewater is notoriously known to contain strong colour, a highly fluctuating pH and significant COD (Chemical Oxygen Demand) values. Because of these characteristics, treatment of these effluents has been rather difficult. Traditional methods for dealing with textile wastewater consist of various combinations of biological, physical and chemical methods. Because of the large variabili...

Morphological and structural properties of layered Au, Pt-YSZ mixed-potential gas sensing electrodes (APE) prepared under different temperature treatments were studied by environmental scanning electron microscope (ESEM) and glow-discharge optical emission spectroscopy (GD-OES), and correlated with open-circuit potential (OCP) and cyclic voltammetry (CV) measurements under gas exposures at elev...

Deposition and stripping of lead ions at thiol based disorganised monolayer modified gold piezoelectrodes was studied by cyclic voltammetry (CV) and electrochemical quartz crystal nanobalance (EQCN). Gold electrodes modified with 3-mercaptopropionic acid and 1,3-dimercapto propane sulphonic acid were studied. Due to the proximity of the potentials for the Pb deposition and thiol reductive desor...

Interference by human plasma proteins in the radioimmunological determination of somatostatin was eliminated by subjecting plasma samples to acid--ethanol precipitation. The assay was performed on the lyophilized supernate from 300 microliters of human plasma, with reagents that are commercially available. Sensitivity was 2.6 pg, corresponding to 8.7 ng/L of plasma. The intra-assay CV was 8%; t...

Poly(3,4-ethylenedioxythiophene) (PEDOT) films were prepared by electro-oxidation on Au microelectrodes in an aqueous solution. Electrolyte solutions and polymerization parameters were optimized prior to overoxidation. The effect of overoxidation time has been optimized by cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS), which results in the film overoxidized for 45 s a...

Carbon nanotubes uniformly 50 nm in diameter were directly grown on graphite foil. Cyclic voltammetry (CV) shows that the carbon nanotube /graphite foil electrode has a high specific capacitance (115.7 F/g at a scan rate of 100 mV/s) and exhibits typical double-layer behavior. A rectangular-shaped CV curve persists even at a scan rate of 100 mV/s in 1.0 M H SO aqueous solution, which suggests t...

Disposable screen-printed nickel/carbon composites on indium tin oxide (ITO) electrodes (DSPNCE) were developed for the detection of glucose without enzymes. The DSPNCE were prepared by screen-printing the ITO substrate with a 50 wt% nickel/carbon composite, followed by curing at 400 °C for 30 min. The redox couple of Ni(OH)₂/NiOOH was deposited on the surface of the electrodes via cyclic volta...