نتایج جستجو برای: crystallite size

تعداد نتایج: 556425  

Journal: :Chemical communications 2015
Peng Li Rachel C Klet Su-Young Moon Timothy C Wang Pravas Deria Aaron W Peters Benjamin M Klahr Hea-Jung Park Salih S Al-Juaid Joseph T Hupp Omar K Farha

The synthesis of nano-sized particles of NU-1000 (length from 75 nm to 1200 nm) and PCN-222/MOF-545 (length from 350 nm to 900 nm) is reported. The catalytic hydrolysis of methyl paraoxon was investigated as a function of NU-1000 crystallite size and a significant enhancement in the rate was observed for the nano-sized crystals compared to microcrystals.

Journal: :Acta Crystallographica Section A Foundations of Crystallography 2005

2008
S. GEORGESCU

YVO4:Eu nanocrystals synthesized by direct precipitation reaction. The morphologic transformation of the nanocrystals as the results of thermal treatments were analyzed using optical spectroscopy. A red shift of the fluorescence lines with the increase of the crystallite size was observed. The kinetics of the D0 level of Eu3+ is also analyzed.

2002
Davor Balzar Nicolae C. Popa

We propose two improvements to the microstructural modeling in Rietveld refinement. The first is the model that yields the complete texture-weighted strain and stress tensors as a function of crystallite orientations, as well as the average values of macroscopic strain and stress tensors for all Laue classes. Implementation in the Rietveld refinement program can be made through the set of refin...

2013
Fahmida Gulshan Kiyoshi Okada

Fe2O3-Al2O3 compounds with different Fe/Al compositions were synthesized by coprecipitation (CP) method and calcined at 300°-1000°C. The formation of crystalline phases (e.g., maghemite, hematite), transformation temperature, specific surface area, lattice parameter, crystallite size, magnetic properties of iron oxide were all affected by the component ratio and thermal treatment.

Although Cu and Fe are immiscible under equilibrium conditions, they can form supersaturated solid solutions by mechanical alloying. In this paper, nano-structured of the metastable Cu-Fe phase containing 10, 15, 20 and 25% wt Fe were synthesized by intensive ball milling for 15h, in order to achieve a solid solution of Fe in Cu. The phase composition, dissolution of the Fe atoms into the Cu ma...

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