نتایج جستجو برای: اسپکتروسکوپی nmr

تعداد نتایج: 59951  

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه شهید چمران اهواز - دانشکده علوم 1371

دراین تحقیق ترکیب داروئی stachydrine از گیاه لگجی با نام لاتین spinosa capparis از خانوادهcapparidacea استخراج گردید.نمونه های مورد آزمایش برگ ، میوه رسیده، میوه نارس این گیاه بود که از منطقه ملاثانی واقع در 35 کیلومتری شمال شهرستان اهواز جمع آوری گردید.استخراج استاچیدرین از طریق چهار روش الف ، ب ،ت و ج، انجام گردید و درپایان این چهار روش را مقایسه نموده و روش ت بعنوان بهترین روش استخراج مشخص ش...

پایان نامه :دانشگاه آزاد اسلامی - دانشگاه آزاد اسلامی واحد تهران مرکزی - دانشکده علوم پایه 1390

یکی از روش های سنتز ترکیبات هتروسیکلی جدید و ایلید فسفر، واکنش تیواوره و مشتقات آن با نمک های تری فنیل فسفین با استیلن های کم الکترون می باشد. هترواتم های گوگرد و نیتروژن در این ترکیبات سنتزی جدید وجود دارند. ساختار محصولات توسط روش های مختلف اسپکتروسکوپی nmr و ir و آنالیزهای عنصری شناسایی شده اند. براساس تحقیقات انجام شده، ترکیبات سنتزی مشابه در داروهای مهمی به ویژه در بیماری های سرطان کاربرد ...

2010
Augusta Caligiani Gerardo Palla Annalisa Maietti Martina Cirlini Vincenzo Brandolini

1H NMR spectra were recorded of methanolic extracts of seven soybean varieties (Glycine max.), cultivated using traditional and organic farming techniques. It was possible to identify signals belonging to the groups of amino acids, carbohydrates, organic acids and aromatic substances in the spectra. In the aromatic zone, the isoflavone signals were of particular interest: genistein, daidzein, g...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2007
Chul Won Kwak Dong-Ho Choung Sung Ran Min Suk Weon Kim Jang R Liu Hoeil Chung

The utility of infrared (IR) spectroscopy for the determination of strawberry ripeness has been successfully demonstrated. Transmission IR spectra were collected using dried liquid extracts from strawberry flesh. The overall IR feature provided fairly noticeable differences, and the ripeness stage was clearly identified using principal component analysis (PCA). Although all of the extracted com...

Journal: :iranian journal of pharmaceutical research 0
abdul majid ayatollahi phytochemistry research center and school of pharmacy, shahid beheshti university of medical sciences, tehran, i.r. iran. seyed mohammad zarei department of pharmacognosy, school of pharmacy, shahid beheshti university of medical sciences, tehran, i.r. iran. arash memarnejadian department of hepatitis and aids, institute pasture of iran, tehran, i.r. iran. mustafa ghanadian department of pharmacognosy, isfahan faculty of pharmacy, isfahan university of medical sciences, isfahan, i.r. iran. mohammad heydarian moghadam department of audiology, school of rehabilitation, shahid beheshti university of medical sciences, tehran, i.r. iran. farzad kobarfard department of medicinal chemistry, school of pharmacy, shahid beheshti university of medical sciences, tehran, i.r. iran.

phytochemical investigation of the aerial parts of euphorbia erythradenia bioss. (euphorbiaceae), one of iranian endemic euphorbias, with particular attention to triterpene constituents, using methanol solvent extraction was carried out. five known triterpenes, including four cycloartanes and oleanolic acid, were isolated for the first time and identified using nmr and mass techniques. anti hiv...

Journal: :iranian journal of pharmaceutical research 0
yucel kadioglu department of analytical chemistry, faculty of pharmacy, ataturk university, 25240, erzurum, turkey. alptug atila department of analytical chemistry, faculty of pharmacy, ataturk university, 25240, erzurum, turkey. mehmet gultekin department of chemistry, faculty of science, ataturk university, 25240, erzurum, turkey. nurdan alcan alp department of chemistry, faculty of science, ataturk university, 25240, erzurum, turkey.

the forced degradation study of lidocaine hcl was carried out according to the ich guideline q1a (r2). the degradation conditions were assessed to be hydrolysis, oxidation, photolysis and dry heat during 24 h, 48 h and 72 h and then the samples were investigated by gc-fid method and nuclear magnetic resonance (nmr) spectroscopy. according to these results, the degradation products were not obse...

Journal: :international journal of nano dimension 0
mehrnoosh khaleghian department of chemistry, islamshahr branch, islamic azad university, tehran, iranسازمان اصلی تایید شده: دانشگاه آزاد اسلامی علوم و تحقیقات (islamic azad university science and research branch) fatemeh azarakhshi department of chemistry, varamin-pishva branch, islamic azad university, varamin, iranسازمان اصلی تایید شده: دانشگاه آزاد اسلامی علوم و تحقیقات (islamic azad university science and research branch)

in this study, b12n12 nano ring has been selected because it consist of four 6-side rings and polar bonds b-n which in comparison with non-polar bonds c-c, is more suitable for the study of the absorption of other compounds. so reactivity and stability of benzene alone and in the presence b12n12 nano ring field checked. to determine the non-bonded interaction energies between benzene and b12n12...

ژورنال: :روش های هوشمند در صنعت برق 2015
کوروش اصلان صفت غلامرضا لطیف شبگاهی

درخت عیب یک دیاگرام سلسله مراتبی است که راههای مختلف ترکیب اجزای معیوب یک سیستم را که منجر به وقوع عیب نامطلوب مشخص در آن می شوند به تصویر می کشد. این دیاگرام در فازهای طراحی و بهره برداری سیستم های صنعتی به کار رفته و به طراحان امکان ارزیابی ویژگی هایی نظیر قابلیت اطمینان، میانگین زمان تا خرابی و حساسیت را عرضه می کند. علاوه بر موارد مذکور از درخت عیب برای پیدا کردن گلوگاه های خرابی و تعیین نق...

Journal: :international journal of nano dimension 0
ashraf sadat ghasemi department of chemistry, payame noor university (pnu), p.o. box,19395-4697, tehran, islamic republic of iranسازمان اصلی تایید شده: دانشگاه پیام نور تهران (payame noor university) ehsan binaeian chemical engineering department, qaemshahr branch, islamic azad university, qaemshahr, iranسازمان اصلی تایید شده: دانشگاه آزاد اسلامی علوم و تحقیقات (islamic azad university science and research branch) habibollah tayebi textile engineering department, qaemshahr branch, islamic azad university, qaemshahr, iranسازمان اصلی تایید شده: دانشگاه آزاد اسلامی علوم و تحقیقات (islamic azad university science and research branch) yasna modanlou jouybari department of chemical engineering, qaemshahr branch, islamic azad university, qaemshahr, iranسازمان اصلی تایید شده: دانشگاه آزاد اسلامی علوم و تحقیقات (islamic azad university science and research branch)

adsorption of co2 on the surface of single-wall zigzag (5,0) and armchair (4,4) carbon nanotubes (swcnts) were studied through using density functional theory (dft) calculations. optimizations of geometric were performed at the b3pw91 level of 6-311++g** method standard basis set using gaussian 03 package of program [1]. structural models were optimized and adsorption energies, band gap, charge...

Journal: :journal of physical and theoretical chemistry 0
mehrnoosh khaleghian department of chemistry, islamshahr branch, islamic azad university, islamshahr, iran fatemeh azarakhshi department of chemistry, varamin-pishva branch, islamic azad university, varamin, iran masoome sheikhi department of chemistry, gorgan branch, islamic azad university, gorgan, iran

to investigate non-bonded interaction of phenanthrene and bn nanostructure, geometric structure of phenanthrene and b12n12 nano-ring with b3lyp method and 6-31g* basis set are optimized by using ab initio gaussian quantum chemical package. the main purpose of this study was to evaluate changes of electronic properties of aromatic compound in presences nano ring field. therefore reactivity and s...

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