The Soft X-ray Undulator beamline at the NSLS supports a soft x-ray imaging program including scanning transmission microscopy, scanning photoemission microscopy, Gabor and Fourier transform holography, and large angle diffraction. Zone plates from an LBL Center for X-ray Optics/IBM collaboration are used as optical elements. The current instrumentation of the beamline and the experimental stat...

sulfated titania nanoparticles (so42-/tio2 nps) were synthesized using titanium tetraisopropoxide (ttip) by the sol-gel method. the structure and morphology of the prepared nanocatalyst was characterized using x-ray diffraction (xrd), scanning electron microscopy (sem) and brunauer–emmett–teller (bet) methods as well as fourier transform infrared (ft-ir) and energy dispersive x-ray (edx) spectr...

the photocatalytic coatings were prepared via incorporating the modified titania nanoparticles into epoxy-based inorganic-organic hybrid coatings. titania nanoparticles were first synthesized from tetra-n-butyl titanate using sol-gel methods by two different calcination treatments, i.e., in mild condition (80°c) and 500°c. the formed anatase nanoparticles were further modified as titania-silica...

using a wide range of techniques, including differential scanning calorimetry, x-ray diffraction, rapid visco analyser and fourier transform infera red spectroscopy, some physicochemical properties of the starch fraction of six iranian rice cultivars (tarom, tarome hashemi, neda, ramezani, fajr and kamfirouzi) [1]were studied and compared. dsc data showed that starch granules of different rice ...

biocl microflowers were synthesized using bismuth nitrate pentahydrate and sodium chloride by microwave (mw) assisted synthesis method for 23 minutes at 180 w. scanning electron microscopy (sem) studies revealed a unique morphology of flower-like assemblies comprised of nanosheets. the x-ray diffraction (xrd) pattern showed that a highly pure and crystalline phase has been obtained. the energy ...

the purpose of the present study was to synthesize and characterize nanosilica from alkali-extraction of silica fume under controlled conditions using poly (vinyl alcohol) (pva) as a dispersing agent. the dissolution efficiency of silica fume was affected by various factors such as concentration of the reagent, reaction time and temperature. a maximum dissolution efficiency of 91% was achieved ...

the zinc-cadmium oxide (zno-cdo) nanocomposites with different weight percentages of cadmium oxide (cdo) nanoparticles were successfully synthesized by the sonochemical method using zinc and cadmium nitrates as precursors to probe their nano-structured surfaces for the decomposition reactions of chloroethyl phenyl sulfide (ceps) as a surrogate of sulfur mustard agent simulant. scanning electron...

in this work, we report high biological performance of silicon substituted nano hydroxyapatite (nha) prepared by immersion of calcium phosphate and sodium silicate as precursors in simulated body fluid (sbf) solution for 24, 36, 48 and 72 hrs at 37°c. characterization and chemical analysis of the synthesized powders were performed by fourier transform, infrared spectroscopy (ft-ir), x-ray powde...

Stoichiometric tetragonal Bal-xSrxTiO3 (x = 0.23) nanopowders were prepared by stearic acid gel(SAG) method using barium stearate, strontium stearate, tetrabutyl titanate as Ba, Sr, Ti sourcesand stearic acid as complexing reagent. Thermal analysis including differential thermogravimetric(DTG) and TG, Fourier transform infrared spectrometry (FTIR), X-ray diffraction (XRD) andtransmission electr...

The crystal structure and chemical bonding of magnetron-sputtering deposited nickel carbide Ni₁-xCx (0.05 ⩽ x⩽0.62) thin films have been investigated by high-resolution x-ray diffraction, transmission electron microscopy, x-ray photoelectron spectroscopy, Raman spectroscopy, and soft x-ray absorption spectroscopy. By using x-ray as well as electron diffraction, we found carbon-containing hcp-Ni...