this paper presents a systematic study of the surface chemistry, porous texture and adsorptive characteristics of prepared new activated carbon using persian mesquite grain. several techniques and methodologies such as, proximate analysis, n2 adsorption–desorption isotherms, scanning electron microscope (sem), fourier transform infrared spectroscopy(ft-ir), x-ray diffraction (xrd), x-ray photoe...

limn2o4 spinel cathode materials have been successfully synthesized by solid-state reaction. surface of these particles were modified by nanostructured lifepo4 via sol gel dip coating method. synthesized products were characterized by thermally analyzed by thermogravimetric and differential thermal analysis(tg/dta), x-ray diffraction (xrd), scanning electron microscopy (sem), and energy dispers...

the catalytic oxidation of toluene over copper oxide supported on natural diatomite was investigated. the catalyst was prepared by the wet impregnation method and characterized by using the brunauer emmett teller (bet), field emission scanning electron microscopy (fesem), x-ray diffraction (xrd), x-ray fluorescence (xrf) and temperature-programmed reduction (tpr) analysis. the highest catalytic ...

copper vanadate nanostructures were prepared via ex-situ precipitation approach in presence of schiff-base ligand (n,n׳ -buthylenebis(acetylacetone iminato)dianion = acacbn) as a new capping agent. the effect of different cu sources and ph on the size, morphology and size distribution of copper vanadate nanostructures was investigated. the as-prepared products were characterized using x-ray dif...

nanocrystals of zno were prepared by microwave irradiation using zn (ii) acetate and triethanol amin (tea) as the starting materials and water as solvent. the nanocrystals of zno with hexagonal (wurtzite) structure were characterized by x-ray powder diffraction (xrd), transmission electron microscopy (tem), scanning electron microscopy (sem), uv-vis absorption and ftir spectroscopy techniques.

in this paper, cuo nanoparticles  have been synthesized via solid-state thermal decomposition using copper(ii) schiff base complexes as new precursors at 600ºc under air atmosphere for 3 h. surface morphology of the products were characterized by fourier transform infrared spectroscopy (ft-ir), x-ray diffraction (xrd) and scanning electron microscopy (sem).

the purpose of the current research is investigating the phenylalanine removal by using magnetic nanoparticles (fe3o4) from water samples. the effect of ph, contact time and phenylalanine concentration on phenylalanine adsorption efficiency by magnetite nanoparticles are studied in a batch system. transmission electron microscopy (tem), x-ray diffraction patterns (xrd) and fourier transform inf...

Heterogeneous catalysis performed in the liquid phase is an important type of catalytic process which is rarely studied in situ. Using microfocus X-ray fluorescence and X-ray diffraction computed tomography (μ-XRF-CT, μ-XRD-CT) in combination with X-ray absorption near-edge spectroscopy (XANES), we have determined the active state of a Mo-promoted Pt/C catalyst (NanoSelect) for the liquid-phase...

Hydrothermal and commercial barium titanate powders were examined for undesirable impurity phases. Compositional differences in the powder were evaluated using x-ray diffraction ( XRD ), x-ray fluorescence ( XRF ), and x-ray photoelectron spectroscopy (XPS). A brium-rich impurity phase, virtually undetectable by XRD, was detected via XPS. Barium impurity phase peaks were detected at binding ene...

Single crystalline zinc oxide (ZnO) nanowires have been grown on Si (100) substrates by a vapor-liquid-solid (VLS) process at temperatures in the range 850-950 °C in an inert atmosphere. The VLS-grown ZnO nanowires have been characterized in detail using X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), X-ray photoelectron spectroscopy (XPS), transmission electron mi...