نتایج جستجو برای: x ray diffraction method
تعداد نتایج: 2226070 فیلتر نتایج به سال:
In this research we report synthesis of new Barium- Cobalt precursor complex with 2,6- pyridine dicarboxylic acid (dipic).Thecomplex[Ba(H2O)6][Co(dipic)2[(1)has been characterized using spectral methods (FT-IR, UV–Vis),elemental analysis and Cyclic voltammetric (CV) method. Also in this study we report thermal decomposition of inorganic precursor complex of (1).Characterization of the binary ox...
In this paper, the bismuth vanadate (BiVO4) nanoparticles were synthesized at 600 °C calcination temperature by co-precipitation method. To study the crystal structure, morphology, optical and photocatalytic properties of the samples, the X-ray diffraction analysis, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, Fourier-transform infrared spectroscopy and ult...
The aim of this research is to investigate different X-ray based quantitative phase analysis methods for determination of cristobalite phase content in ceramic cores. For this purpose, four popular routes including peak absolute intensity method, relative intensity ratio method, direct or calibration method and internal standard (or Alexander-Klug) method have been chosen. Some control samples ...
Structural information about biological macromolecules near the atomic scale provides important insight into the functions of these molecules. To date, X-ray crystallography has been the predominant method used for macromolecular structure determination. However, challenges exist when solving structures with X-rays, including the phase problem and radiation damage. X-ray-free electron lasers (X...
The x-ray standing wave method ~XSW! and high-resolution x-ray diffraction were used to study the structural perfection and polarity of GaN epitaxial thin film grown by hydride vapor phase epitaxy on the Si-face SiC substrate. The x-ray standing wave was generated inside the 300 nm thin film under the condition of Bragg diffraction from the film. Excellent crystalline quality of the GaN film wa...
Coherent x-ray diffraction microscopy is a method of imaging nonperiodic isolated objects at resolutions limited, in principle, by only the wavelength and largest scattering angles recorded. We demonstrate x-ray diffraction imaging with high resolution in all three dimensions, as determined by a quantitative analysis of the reconstructed volume images. These images are retrieved from the three-...
calcium fluoride nanoparticles with special amount of cerium ion (%1) were synthesized by coprecipitation. fourier transforms infrared spectroscopy (ftir), x-ray diffraction (xrd), absorption and photoluminescence (pl) from caf2ce nanoparticles has been investigated. ftir spectra reveal that there are some amounts of oh, no3 and other organic functional groups on the particle surfaces before th...
in the present work, bi2s3 nanostructures have been synthesized with the aid of thioglycollic acid (tga) a solvent, capping agent, and sulfide source in the presence of ultrasonic method. the as-synthesized products were characterized by x-ray diffraction (xrd), energy dispersive x-ray spectroscopy (eds), scanning electron microscope (sem), and photoluminescence (pl) spectroscopy. the band gap ...
in the current paper,nanostructured nickel oxide (nio) were synthesized by co-precipitation method using nickel(ii) chloride hexahydrate (nicl2.6h2o) and sodium hydroxide (naoh) as starting material. structural, optical and magnetic properties of nanostructures were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), atomic force microscope (afm), uv–vis absorption; fo...
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