Covalent organic frameworks (COFs) are typically synthesized using solvothermal conditions (>120 °C, >72 hours) in harmful solvents. Here we report a strategy to rapidly (<60 minutes) synthesize imine-linked COFs aqueous acetic acid sonochemistry and thus avoid most of the disadvantages methods. Using sonochemical method, our knowledge previously unreported COFs. The crystallinity porosity thes...