نتایج جستجو برای: solvothermal method
تعداد نتایج: 1631216 فیلتر نتایج به سال:
Brominated flame retardants (BFRs) in electrical and electronic (E&E) waste plastic are toxic, bioaccumulative and recalcitrant. In the present study, tetrabromobisphenol A (TBBPA) contained in this type of plastic was tentatively subjected to solvothermal treatment so as to obtain bromine-free plastic. Methanol, ethanol and isopropanol were examined as solvents for solvothermal treatment and i...
A rapid detection method of Pseudomonas aeruginosa based on magnetic separation and chemiluminescence was developed in this paper. Magnetic nanoparticles (MNPs) were prepared by solvothermal method with PEG-4000 as a surfactant, and then were modified. The prepared MNPs present a uniform morphology and good dispersion. The sizes of MNPs can be controlled by adjusting the dosage of FeCl3 x 6H2O....
Hexagonal phase (β) sodium rare earth tetrafluorides (NaREF4, RE = Y, Gd, Lu, et al.) are considered the ideal matrices for lanthanide (Ln) ions doped upconversion (UC) luminescence materials, because they can provide favorable crystal lattice structures for the doped luminescent Ln ions to make intensive emissions. However, the cubic phase (α) NaREF4 always preferentially forms at low reaction...
graphene-based nanocomposites are newly emerged materials with a wide range of applications such as in supercapacitors electrode. the high conductivity and ability for passing electric current, makes graphene an appropriate new item to be used in cells. electroactive transition metal oxides, owing fast reversible redox pairs, are used to store electrical charge. furthermore, the graphene/nio na...
Although nanosizing Li4Ti5O12 (LTO) materials is an effective way to improve their rate performances, their low tap density and first cycle coulombic efficiency limit their practical applications. To tackle these problems while preserving the advanced rate performances, monodispersed mesoporous LTO submicrospheres are developed here. These submicrospheres are synthesized via a solvothermal meth...
Deposition of ZnO nanorod films using a simple solvothermal method with narrow fluorescence emission due to defects is exemplified. The synthesized thin show excellent potential for UV detection. Their optical properties reflect their semiconducting nature as expected.
Herein, we report a facile surfactant-assisted solvothermal synthetic method to prepare nearly monodisperse spherical CeO(2) nanocrystals. A good control of the size of CeO(2) nanocrystals in the range of 100-500 nm was achieved by simply varying the synthetic parameters such as reaction time, volume ratio of ethanol to water (R), molar ratio of PVP, and concentration of Ce(NO(3))(3)⋅6 H(2) O i...
Time-resolved in situ SAXS and XAS measurements were carried out to monitor the formation of nanoparticles of the sulfides of cadmium and zinc, from solutions containing he corresponding acetate, and thioacetamide under solvothermal conditions. Analysis of the SAXS data shows that particles of ca 5 nm in radius form within the first few minutes of the reaction and then grow uniformly to ca 20 n...
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