Traditional hydrodistillation (HD), steam distillation extraction (SD), organic solvent extraction (SE), and microwave assisted hydrodistillation (MWHD) techniques were compared and evaluated for their effectiveness in the isolation of essential oil of Melissa officinalis from Algeria. The microwave assisted hydrodistillation technique was optimized in terms of both delivered power and time dur...

The kinetics of polyphenol extraction from brewer's spent grain (BSG), using a batch system, ultrasound assistance, and microwave assistance and the evolution of antioxidant capacity of these extracts over time, were studied. The main parameters of extraction employed in the batch system were evaluated, and, by applying response surface analysis, the following optimal conditions were obtained: ...

The purpose of this study was to extract phenolic compounds from olive leaves of Koroneiki, Roghani and Mission varieties by maceration and Microwave-assisted extraction (MAE) methods with different solvents. Our results revealed that the extraction method, solvent and variety had a significant effect on the amount of phenolic compounds (p<0.05). In both extraction methods, Koroneiki and Missio...

since solid-phase and liquid-phase microextraction (spme and lpme) were introduced, as effective solvent-free methods, many efforts have been made to improve their modes and applications. however, due to limitations with sensitivity and efficiency, researchers have focused on improving the performance of their basic primary modes. in this way, in recent years, different methods such as ultrason...

A simple and rapid microwave-assisted extraction (MAE) procedure has been developed and optimized for extracting triterpenoids (TTP) from the Actinidia deliciosa root. Several variables that could potentially affect the extraction efficiency, namely extraction time (min), ethanol fraction (%), liquid:solid ratio (volume per mass) and microwave power (W) have been optimized by means of response ...

A suitable methodology of synthesis of coumarin derivatives by Pechmann reaction over heterogeneous solid acid catalysts in a free solvent media under microwave irradiation is described. Resorcinol, phenol and ethyl acetoacetate were selected as model reactants in the Pechmann condensation. The catalytic activity of several materials-Amberlyst-15, zeolite β and sulfonic acid functionalized hybr...

The objective of this research was to develop, optimize, and validate a modern, rapid method of preparation of human hair samples, using microwave irradiation, for analysis of eight tricyclic antidepressants (TCADs): nordoxepin, nortriptyline, imipramine, amitriptyline, doxepin, desipramine, clomipramine, and norclomipramine. It was based on simultaneous alkaline hair microwave-assisted hydroly...