the austenitic stainless steel (ss) has been used as a material for  building  ultra  high  vacuum  (uhv)  chamber.  recently significant  efforts  have  been  concerned  a  comparing  the standard  cleaned  for  ultra  high  vacuum,  passivity  stainless. in  this work austenitic  nanocomposites were  synthesize by sol-  gel method. the morphologies  and  topographies  of  the samples  have  b...

the dried nitrate-urea gels exhibit the combination of autoicatatric combustion behavior and ultrasonic, whichcan be used to synthesize the nanocatalyst ferrite powders. cu and ni unites nanocatalyst powders sithcomposition of caned], and nife204 were synthesized by a sol-gel auto catalnic combustion process. themolar ratio between metal ions and urea was 11.2. the sob gel process was done at 8...

The implications of organically-modified silica-based materials in electrochemical science is reviewed along with some selected recent trends in the field of functionalized and sol–gel silica electrochemistry. These recent trends include the electro-assisted generation of organosilica films on solid electrode surfaces, the preparation and applications of sol–gel derived composite (carbon, gold,...

We report on the fabrication and characterization of thick UV-patternable hybrid sol-gel films by spin coating using a modified sol-gel process. Thick coating of 25 microns with crack-free surface can be produced by one spin coating step. Thick layers of more than 100 μm can be obtained with a multi-coating process. Characterization using different techniques including optical microscope and at...

Polvos cerámicos de Sm2O3 dopados y mezclados con europio se obtuvieron a partir la formación cloruros samario través ruta sol-gel citrato. Este trabajo reporta influencia los iones en las propiedades estructurales luminiscentes cerámicas Sm2O3:Eu3+ (coordenadas CIE) variando el Eu3+ 10 50% mol. Las características químicas, morfológicas fueron establecidas por FTIR XRD, revelando presencia ban...

The doping of porous sol-gel films by adsorption of cations onto silica from aqueous solutions is demonstrated. The films are fabricated using the sol-gel method, giving nanometer scale porosity, high surface area, and homogeneity on the scale of optical wavelengths. After deposition by spin coating and initial heat treatment, the films are soaked in a salt solution of the desired dopant, and t...

Bioencapsulation of microbial cells in silica-based matrices has proved to be a good strategy to enhance the biosynthetic capabilities and viability of bioproducers. In the present study, mycelium and pellet cultures of strain Aspergillus oryzae PP were successfully immobilized in sol-gel hybrid matrices composed of tetraethylorthosilicate as an inorganic precursor, 5% (w/v) starch and 10 or 15...

high purity lead titanate nanopowders in tetragonal form have been successfully prepared bycitric acid gel method using lead nitrate and tetra-n-butyl titanate as pb and ti sourcesrespectively and citric acid as complexing reagent. the precursors were calcined at varioustemperatures ranging from 450 °c to 600 °c for 2 h. fourier transform infraredspectroscopy (ft-ir), x-ray diffraction (xrd) an...

Parameters and/or processes responsible for the stability of catalyst supports and ceramic membranes are discussed. Two major parameters/processes were identified which are responsible for the stabiliv of sol-gel derived nanostmctured oxides at elevated temperatures. They are metastable-to-stable phase transformation and structure and packing of primary particles within the aggregate. Based on ...