Tungsten (W) was coated onto a silicon (Si) anode at the nanoscale via the physical vaporization deposition method (PVD) to enhance its electrochemical properties. The characteristics of the electrode were identified by scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray analysis, and electron probe X-ray microanalysis. With the electrochemical pr...

synthesis, identification and thermal behavior studies of nanoparticles cobalt (ii) bromide has been studied in this research. cobalt (ii) bromide was synthesized by planetary high-energy ball mill. the general formula of this compound is cobr2.6h2o. the synthesized nanoparticles were characterized by fourier transform infrared spectroscopy and also size and structure of synthesized nanoparticl...

co-fe films were electrodeposited on cu substrate from electrolytes with different co concentration  levels. x-ray diffraction (xrd) was used  to  investigate  the  films  crystal  structures. the  results  indicate that  if  the  co  concentration  is  less  that  the  fe  concentration,  the cubic  structure  appears  in  the  films, while  the  hexagonal  structure dominates when  the co  co...

The Transition Edge Sensor (TES)-Energy Dispersive Spectrometer (EDS) is an X-ray detector with high-energy resolution (12.8 eV). The TES can be mounted to a scanning electron microscope (SEM). The TES-EDS is based on a cryogen-free dilution refrigerator. The high-energy resolution enables analysis of the distribution of various elements in samples under low acceleration voltage (typically unde...

We have developed an automated data analysis method for atmospheric particles using scanning transmission X-ray microscopy coupled with near edge X-ray fine structure spectroscopy (STXM/NEXAFS). This method is applied to complex internally mixed submicrometer particles containing organic and inorganic material. Several algorithms were developed to exploit NEXAFS spectral features in the energy ...

In this work, PbSe and PbTe sensitized TiO2 solar cells were fabricated. PbSe and PbTe nanostructure was deposited on the TiO2 surface via a drop cast method. The fabricated surfaces were examined by atomic force microscopy (AFM). Also the optical properties of the layers were studied by diffuse reflectance spectroscopy (DRS) spectra. The morphology of the surfaces was obtained by scanning elec...

Intermetallide phase formation was studied in a powdered Fe–Al system under layer by layer laser cladding with the aim of fabricating the gradient of properties by means of changing the Fe–Al concentration ratio in the powder mixture from layer to layer. The relationships between the laser cladding parameters and the intermetallic phase structures in the consecutively cladded layers were determ...

This paper describes synthesis of In2S3 nanoparticles by sonochemistry method and their application to enhance solar cells performance which In2S3 nanoparticles work as co-sensitizer for the first time. In2S3 is a narrow band gap semiconductor (2 eV) with conduction band higher than TiO2. Therefore it can transfer electron to the conduction band of TiO2. The effect of different parameters such ...

The purpose of this study was to fabricate and investigate the highly porous structure using titanium dioxide, which is a candidate for bone defect repairing. For this purpose, TiO2 scaffolds were synthesized using titanium butoxide, Pluronic F127 surfactant, and polyurethane foam blocks. Therefore, a colloid includes titanium butoxide and F127 and the polyurethane foams were immersed in it. Th...

the corrosion protection abilities of modified copper in 2-[((z)-1-{6-[(2-sulfanylphenyl)ethanimidoyl]-2-pyridyl}ethylidene)  amino]-1-benzenthiol solution containing tio2 nanoparticles were evaluated by tafel  polarization  and  impedance  spectroscopy  in  3.5%  sodium chloride  solution.  the  samples  were  characterized  by  energy dispersive  x-ray  (edx)  and  scanning  electron  microsc...