Microwave assisted combustion synthesis is used for fast and controlled processing of advanced ceramics. Single phase and sinter active nano crystalline alpha alumina powders were successfully synthesized by different fuel-to-oxidant molar ratios using aluminium nitrate as an oxidiser, glycine as a reducing agents and millipore water as a solvent by microwave assisted combustion synthesis. Ther...

This article describes the recent research progress in the field of crystalline metal-chalcogenide superlatticescontaining tetrahedron-shaped nanoclusters as building units. With the development of new synthetic strategies and structuralconcepts, new clusters that are members of three series of tetrahedral clusters (i.e., supertetrahedral clusters, pentasupertetrahedralclusters, and...

The research and development of solid state gas sensors with low cost and reduced size for the monitoring of the gaseous species is rapidly increasing in the last years [1]. Many technological approaches have been proposed regarding the different materials and the detecting principles. The currently available sensors use several transduction principles: thermal, mass, potentiometric, amperometr...

The challenge of estimating the crystalline-fraction of dense randomly-oriented nano-particles, contained in a (less-dense) amorphous support, is increasingly important in fields as diverse as heterogeneous-catalyst design and electronic-data storage. Lattice-fringe visibility-analysis [1,2] is a potential tool in this context, but of course interfering contrast from the amorphous support (as w...

We report on the formation of a stable Body-Centered Heptahedral (BCH) crystalline nanobridge structure of diameter ~ 1nm under high strain rate tensile loading to a <100> Cu nanowire. Extensive Molecular Dynamics (MD) simulations are performed. Six different cross-sectional dimensions of Cu nanowires are analyzed, i.e. 0.3615 x 0.3615 nm, 0.723 x 0.723 nm, 1.0845 x 1.0845 nm, 1.446 x 1.446 nm,...

a  facile  effective  stirring  aging  at  room  temperature  prior  to  conventional  hydrothermal treatment was employed in the template-free synthesis of micro- and nano-crystalline sodalites with  two  different  initial  gel  compositions.  the  effect  of  initial  si/al  molar  ratio,  naoh concentration and stirring aging time were investigated on the morphology and particle size of the...

zno and mn-zno nano powders were prepared by the sol-gel auto combustion method. the products were characterized by x-ray diffraction (xrd), energy dispersive analysis of x-ray (edx) and scanning electron microscopy (sem). structural and morphological properties of nano particles were investigated and the average crystalline size of zno and mn-doped zno was obtained 44 and 51 nm, respectively. ...

nano zno/ montmorillonite composite were prepared by sol gel method under ultrasonic irradiation from directly mixing montmorillonite nano clay into zinc gel. the zn(ch3coo)2.2h2o and montmorillonite nano clay was used as precursor. the zinc acetate was dissolved in di water and, nh3 (aq) solution was dropped into the zinc solution until ph 9 consequently the zinc gel was produced. the montmori...

Crystalline tantalum thin films of about 500nm thickness were deposited on AISI 316L stainless steel substrate using magnetron sputtering. To investigate the nano-mechanical properties of tantalum films, deposition was performed at two temperatures (25°C and 200°C) on TaNx intermediate layer with different N2/Ar flow rate ratio from 0 to 30%. Nano-indentation was performed to obtain the mechani...

A simple route towards nanostructured mesoporous Indium-Tin Oxide (templated nano-ITO) electrodes exhibiting both high conductivities and optimized bicontinuous pore-solid network is reported. The ITO films are first produced as an X-ray-amorphous, high surface area material, by adapting recently established template-directed sol-gel methods using Sn(IV) and In(III) salts. Carefully controlled ...