Chemical characterization studies for medical devices rely on extract preparation techniques such as liquid–liquid extraction to render the more amenable instrumental analysis. Considering these are generally non-targeted, effect of full range potential analytes must be considered. However, there is currently no workflow evaluating impact non-targeted extractables. Herein, we present a framewor...

The use of liquid-liquid extraction for the separation of tantalum from niobium was demonstrated. Tantalum and niobium spectrographically free of each other were prepared in quantity on a continuous basis.

This paper demonstrated a fluorescence-indicated mass transfer liquid-liquid extraction process based on a droplet microfluidic system. Analysis of the droplet-based liquid-liquid extraction process based on the description of mass transfer into or out of droplets is conducted. The relationship between the extraction efficiency and the droplet size is measured and the mass transfer coefficient ...

The Brønsted acidic ionic liquid ([BMIm]HSO4) catalyzed three-component synthesis of 2H-indazolo[2,1-b]phthalazine-trione derivatives at room temperature. The integrity of the ionic liquid remains reasonably unchanged when it is separated from the reaction mixture by water extraction, as it can be recycled several times without any loss of activity in each of the title syntheses. The products a...

the brønsted acidic ionic liquid ([bmim]hso4) catalyzed three-component synthesis of 2h-indazolo[2,1-b]phthalazine-trione derivatives at room temperature. the integrity of the ionic liquid remains reasonably unchanged when it is separated from the reaction mixture by water extraction, as it can be recycled several times without any loss of activity in each of the title syntheses. the products a...

The extraction behavior of neodymium and other rare earths from nitric acid media by the functionalized ionic liquid trioctylmethylammonium dioctyl diglycolamate, [A336][DGA], was investigated. The nonfluorinated ionic liquid trioctylmethylammonium nitrate, [A336][NO3], was used as diluent. The extraction behavior of neodymium(III) in this ionic liquid solution was carried out as a function of ...

An isocratic high-performance liquid chromatographic method for the determination of testosterone (T) and epitestosterone (ET) in human urine using liquid-liquid or solid-phase extraction (SPE) is developed and validated. The optimum separation is achieved using a Hypersil C(18) column, water-acetonitrile (57:43, v/v) as the mobile phase and UV-absorbance detection at 245 nm. The recoveries obt...

in this study, for the analysis of human urine samples, a novel method explained for the determination of celecoxib, a nonsteroidal anti-inflammatory drug (nsaid), using molecularly imprinted solid-phase extraction (mispe) coupled with high-performance liquid chromatography (hplc). the synthesis of the mip was performed by precipitation polymerization in methacrylic acid (maa), ethylene glycol ...