For long-term pharmacokinetic studies in humans as well as in experimental animals, an analysis of strontium (Sr) with a low detection limit and high sensitivity is necessary. The data presented here describe the optimization of the furnace program and sample handling for measuring Sr in plasma by using graphite furnace atomic absorption spectrophotometry. The method was validated and applied t...

To evaluate the hypothesis that lactation stimulates lead release from bone to blood, the authors analyzed breastfeeding patterns and bone lead concentrations as determinants of blood lead levels among 425 lactating women in Mexico City for 7 months after delivery (1994-1995). The authors measured in vivo patella and tibia lead concentrations at 1 month postpartum using K x-ray fluorescence. Ma...

In the present study, an ultrasound-assisted emulsification microextraction based on solidification floating organic drop method is described for preconcentration of trace amounts of Mn (II). 2-(5-Bromo-2-pyridylazo)-5 diethylaminophenol was added to a solution of Mn(+2) at ph = 10.0. After this, 1-undecanol was added to the solution as an extraction solvent, and solution was stirred. Several f...

This method for determination of Rb+ in human plasma and erythrocytes by graphite-furnace atomic absorption spectrophotometry has a sensitivity of 29 nmol/L for plasma, 12 nmol/L for erythrocytes. The detection limit is 24 nmol/L for plasma, 4.8 nmol/L for erythrocytes. This assay is approximately 30-fold more sensitive than previously reported techniques involving atomic absorption spectrophot...

This study describes and compares two methods of atomic absorption spectrometry (AAS) for the selenium (Se) analysis in food: electrothermal AAS (ET AAS) and hydride generation method of AAS (HG AAS). The accuracy of the two methods was established by analysing two biological reference materials: Wheat Flour 1567a and Bovine Liver 1577b from the National Institute of Standards and Technology, U...

an amoniumvanadate plus sodium molybdate mixed modifier graphite furnace atomic absorption spectrometric method has been developed for determination of traces of lead in drinking water. the concentration of lead in the sample is obtained by direct comparison to linear working graph prepared from aqueous standards in the modifier medium, the results indicate the better performance of the propose...

this study was conducted to determine the residues of mercury (hg), lead (pb), copper (cu) and cadmium (cd) in the imported tilapia fillets. thirty random samples from imported tilapia fillets were collected from different markets in isfahan city, central iran. they were analyzed using graphite furnace atomic absorption spectrometer (perkin elmer 800) for pb, cu, cd and flow injection mercury s...

II for each step of the analysis cycle. At the end of each step the external clock is reset as is the 8 bit control pattern for the next function. The final step is to activate the AA analysis cycle and to wait for the furnace to cool before injection of the next sample. We have found that programming a waiting time longer than the cooling time extends the life of the graphite cuvettes. The pro...

Abstract Anode gas bubble behavior and anode effect on graphite industrial carbon rod-shaped in a cryolite melt have been studied using see-through furnace. The different materials properties which can affect electrochemical properties. Industrial is more inhomogeneous with respect to structure, pore, aggregates impurities comparison the graphite. More bubbles were nucleated than for same curre...

We describe the development of a direct method for determination of selenium in serum by graphite-furnace atomic absorption spectrophotometry with deuterium background correction. We include palladium modifier to stabilize selenium in the presence of a strong reducing agent. Spectral interferences from iron are not evident in this system. Because an analysis requires only 20 microL of serum or ...