the synthesis of titania via sol-gel method has been widely studied. in the present work, titania was deposited onto a titanium substrate via sol-gel method. different processing parameters such as the repetition number of dipping/heat treatment process and dipping time have been studied to obtain the homogenous titania coating. phase and microstructural evaluation of the powder and coating sam...

In this work, sol-gel processing was used to synthesize the fluorohydroxyapatite (nano-FHA, Ca10(PO4)6(OH)2−xFx) nanopowders. The advantages of the sol-gel method over other methods are precise control of composition, low processing temperature, and better homogeneity. Calcium nitrate tetrahydrate, phosphorous pentoxide and Tetrabuthylammon...

In this work, preparation and crystallization of yttrium iron garnet Y3Fe5O12 super-paramagnetic nanoparticle by aqueous sol–gel processes and its application as an effective nano catalyst for esterification and etherification reactions in short reaction time and in high isolated yields. Then this catalist was used for the synthesis of Dihydropyrimidin derivatives is described. The catalyst was...

A simple highly versatile and efficient sonochemical synthesis of 1,2,4,5-tetrasubstituted and 2,4,5-trisubstituted imidazoles is achieved by condensation of 1,2-dicarbonyl compound, aldehyde, ammonium acetate and primary amine using antimony trichloride immobilized on silica gel (SiO2-OSbCl2) as a catalyst in ethanol at moderate temperature. Operational simplicity, practicability and applicabi...

OBJECTIVE To study the effect of interleukin-1 (IL-1) on the synthesis of proteoglycans biglycan (DSPG-I) and decorin (DSPG-II) in intact bovine articular cartilage. METHODS Cartilage bearing sesamoid bones from the metacarpophalangeal joint were cultured with 10 ng/ml IL-1 for 2 days and labelled with [35S] sulfate. One sesamoid bone from each animal had been labelled ex vivo. The remaining ...

A simple highly versatile and efficient sonochemical synthesis of 1,2,4,5-tetrasubstituted and 2,4,5-trisubstituted imidazoles is achieved by condensation of 1,2-dicarbonyl compound, aldehyde, ammonium acetate and primary amine using antimony trichloride immobilized on silica gel (SiO2-OSbCl2) as a catalyst in ethanol at moderate temperature. Operational simplicity, practicability and applicabi...

Abstract Different alumina samples prepared with sol–gel, chemical precipitation and hydrothermal synthesis were used as supports of Fe-promoted Rh-based catalysts for ethanol via CO hydrogenation. The characterized by means N 2 -adsorpotion, XRD, H -TPR, XPS, STEM, -TPD, DRIFTS, chemisorption. results indicated that the Al O 3 exhibited nano-fiber morphology constituted mixed crystal phases, w...

The use of plant extract is generating interest of researchers toward cost effective and eco-friendly green synthesis of nanoparticles. In the present work, Cupric oxide nanoparticles were synthesized using coffee powder extracts by the sol-gel method at different calcination temperatures. The synthesized nanoparticles were characterized by X-ray diffraction, scanning electron microscopy , ultr...