We present a simple and robust method to acquire quantitative maps of compositional fluctuations in nanostructures from low magnification high-angle annular dark field (HAADF) micrographs calibrated by energy-dispersive X-ray (EDX) spectroscopy in scanning transmission electron microscopy (STEM) mode. We show that a nonuniform background in HAADF-STEM micrographs can be eliminated, to a first a...

We report the controlled alloying, oxidation, and subsequent reduction of individual AgAu nanoparticles in the scanning transmission electron microscope (STEM). Through sequential application of electron beam induced oxidation and in situ heating and quenching, we demonstrate the transformation of Ag-Au core-shell nanoparticles into: AgAu alloyed, Au-Ag core-shell, hollow Au-Ag2O core-shell, an...

INTRODUCTION The aim of this study was to investigate the changes in the surface structure and chemical composition after applying bleaching agents to completely hardened mineral trioxide aggregate. METHODS A total of 12 samples of MTA blocks were divided into three groups, two different bleaching agents, and a control group. The surface structure was observed using a scanning electron micros...

The purpose of this study was to investigate the enamel remineralization potential of two toothpastes, one of which was based on Recaldent (CPP- ACP) and the other on NovaMin (Calcium-sodium-phosphosilicate). Human permanent molar teeth were subjected to three consecutive demineralization cycles. These cycles were followed by remineralization of the experimental groups by toothpastes containing...

The aim of this study was to evaluate the effect of rosin upon fixing boron in Styrax tonkinensis (Piere) wood treated with mixtures of 3% boric acid and 1% rosin sizing agent. After treatment, wood samples were also analyzed by scanning electron microscope observation and energy-dispersive X-ray spectroscopy (SEM-EDX). The results showed that all boron-rosin formulations impregnated Styrax ton...

Ultrasonic-assisted green synthesis of silver nanoparticles is gaining more attention owing to its benefits over conventional process. The main objective this study was synthesize with aqueous cinnamon extract using ultrasound-assisted extraction and their physico-chemical characterization. Total phenolic content, DPPH, FRAP were 315 mg GAE/g, 89% scavenging activity 9.5 mmol Trolox eq/100 g re...

Europium (Eu) doped ZnO microsphere based nano-sheets were synthesized through hydrothermal method. Effects of different concentrations of Europium on structural and optical properties of ZnO nano-sheets were investigated in detail. Prepared un-doped and Eu-doped ZnO samples were characterized using X-Ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDX), scanning electron micro...

In₂O₃/SnO₂ composite hetero-nanofibers were synthesized by an electrospinning technique for detecting indoor volatile organic gases. The physical and chemical properties of In₂O₃/SnO₂ hetero-nanofibers were characterized and analyzed by X-ray diffraction (XRD), field emission scanning electron microscope (FE-SEM), Energy Dispersive X-Ray Spectroscopy (EDX), specific surface Brunauer-Emmett-Tell...

Energy-dispersive X-ray microanalysis (EDX) is a technique for determining the distribution of elements in various materials. Here, we report a protocol for high-spatial-resolution X-ray elemental imaging and quantification in plant tissues at subcellular levels with a scanning transmission electron microscope (STEM). Calibration standards were established by producing agar blocks loaded with i...

Copper nanoparticles have been deposited on silicon surfaces by a simple galvanic displacement reaction, and rapid thermal annealing has been performed under various atmospheric conditions. In spite of the general tendency of the agglomeration of nanoparticles to lower the surface energy at elevated temperatures, our plan-view and cross-sectional transmission electron microscopy (TEM), energy d...