A laser-assisted plasma-coating technique at atmospheric pressure (LAPCAP) has been investigated. The electron temperature, electron density and gas temperature of the atmospheric-pressure plasma have been measured using optical emission spectroscopy (OES). LAPCAP utilizes laser ablation of 3 mol% yttria-stabilized zirconia into an atmospheric helium/nitrogen plasma to deposit thermal barrier c...

We develop a solution-based nanoscale patterning technique for site-specific deposition and dissolution of metallic nanocrystals. Nanocrystals are grown at desired locations by electron beam-induced reduction of metal ions in solution, with the ions supplied by dissolution of a nearby electrode via an applied potential. The nanocrystals can be "erased" by choice of beam conditions and regrown r...

The channelspark, a low accelerating voltage, high current electron beam accelerator, has been used for ablation of materials applied to thin film deposition. The channelspark operates at accelerating voltages of 10 to 20 kV with ;1500 A beam currents. The electron beam ionizes a low-pressure gas fill ~10–20 mTorr Ar or N2) to compensate its own space charge, allowing ion focused transport. Abl...

Lithium manganese oxide thin films have been grown using a gas jet based, electron beam directed vapor deposition technique. The deposition rate could be controlled by the electron beam power as well as the gas jet density and speed. This enabled films to be grown at deposition rates up to 16 nm /s which is a significantly higher deposition rate than that reported for the growth of this materia...

Electron beam induced deposition of amorphous carbon finds several uses in microlithography, surface micromachining, and the manufacturing of microand nanomechanical devices. This process also occurs unintentionally in vacuum chambers of electron microscopes and interferes with normal image acquisition by reducing resolution and causing charging effects. In this work, we show that the resonance...

AISI 316 stainless steels were coated with 250 nm Ni film by electron beam deposition and post-annealed at different temperatures with a nitrogen flow of 600 cm3min-1 nitrogen. The prepared samples were corrosion tested in 1.0 M sulphuric acid solution using potentiodynamic technique. Crystallographic and morphological structure of the samples were analyzedanalysed by X-ray diffraction (XRD) an...

Ion implantation is a surface modification technology to produce new material on the surface by impingement of high energy ions from the ion accelerator. In this work, AISI 304 stainless steels were coated with 90 nm Ni film by electron beam deposition and implanted by a flow of 5×1017 N cm−2 at 400 K temperature with different implantation energies of 10, 20, 30 and 40 keV. The prepared sample...

magnesium alloys as biodegradable materials can be used in body as an implant materials but since they have poor corrosion resistance, it is required to decrease their corrosion rate by biocompatible coatings. in this study, hydroxyapatite (ha) coatings in the presence of an intermediate layer of zrn as a biocompatible material, deposited on az91 magnesium alloy by ion beam sputtering method at...

Liquid containing environmental cell based TEM has, in recent years, become a powerful tool for studying dynamic systems at nanometer length scales.[1-7] Such cells typically confine several hundred nanometers of liquid between two electron transparent windows. These cells can be integrated with electrodes for electrochemical testing, and have been implemented to study processes including elect...

NASA’s Langley Research Center and Johnson Space Center are developing a solid freeform fabrication system utilizing an electron beam energy source and wire feedstock. This system will serve as a testbed for exploring the influence of gravitational acceleration on the deposition process and will be a simplified prototype for future systems that may be deployed during long-duration space mission...