Abstract This paper presents the experimental analysis of vulcanization process nitrile rubbers for diaphragms fabrication used in FBG-based pressure sensors. Tests using with different rubber thicknesses (0.5mm, 1.0mm, and 1.5mm), temperatures (125°C, 150°C, 200°C), times (2.5min 5.0min) were performed to analyse chemical degradation diaphragms. Degradation was digital macrography diaphragm su...