نتایج جستجو برای: crystallite refinement
تعداد نتایج: 35490 فیلتر نتایج به سال:
The objective of this work is to study the effect of two key factors external magnetic field and applied current density during template-based electrodeposition of nickel nanowires using an electrode distance of 20 mm. Morphology, length, crystallite size and crystallographic characterization of the grown nickel nanowires at an electrode distance of 20mm are presented. For this electrode distan...
The objective of this work is to utilize a low-grade synthetic rutile to produce high-grade titania nanoparticles. Due to the nature of the precursor, the hydrothermal method needs modification in order to accommodate the precursors and chemical reagents. The product will be characterized with the XRD (crystallite size and crystallinity), EDXRF (chemical composition), SEM (Morphology), N2 adsor...
Microsegregation is one of the most important phenomena occurs during solidification. It usually results in formation of some unexpected second phases which generally affect the mechanical properties and specially reduce the workability of casting products. The aim of this research is to study the effect of cooling rate and grain refinement on the microsegregation in Al-4.8 wt.% Cu. For this p...
Mechanical alloying of Ti-Si and NiTi was performed by high-energy ball milling at ambient temperature. The structural and compositional evolutions during mechanical alloying were investigated. Results showed that the crystallite size of mechanically alloyed Ti-Si and Ni-Ti powders decreased with increasing milling time and the steady-state crystallite size was approximately 10 nm. The mechanic...
In this paper, we have reported convenient way to access CdTe nanorods by solvothermal decomposition using single source molecular precursor cadmium (II) bis-(isopropyl telluro) propane (SSMP) and quinoline as solvent at relatively low temperature (200oC).As synthesized nanomaterials are structurally characterized by XRD, SEM and UVVisible spectroscopy. SEM micrographs revealed formation of rod...
Crystallization represents the prime example of a disorder-order transition. In realistic situations, however, container walls and impurities are frequently present and hence crystallization is heterogeneously seeded. Rarely the seeds are perfectly compatible with the thermodynamically favoured crystal structure and thus induce elastic distortions, which impede further crystal growth. Here we u...
Four different ceria supported catalyst were prepared by impregnation method with Pt(NO3)2 solution. The two supports are commercially available (MaTeck) and the other two were prepared by precipitation and microwave assisted hydrothermal method (MAH) respectively. The phase composition and average crystallite size of the catalysts were characterised with XRD technique. Finally the catalytic ac...
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