نتایج جستجو برای: calcinated

تعداد نتایج: 174  

Nano ZnO/ montmorillonite composite were prepared by sol gel method under ultrasonic irradiation from directly mixing montmorillonite nano clay into Zinc gel. The Zn(CH3COO)2.2H2O and montmorillonite nano clay was used as precursor. The zinc acetate was dissolved in DI water and, NH3 (aq) solution was dropped into the zinc solution until pH 9 consequently the zinc gel was produced. The montmori...

A. Farhadyar M. Zare-Dehnavi N. Farhadyar Sh. Aghabeygi,

Nanocomposite of ZrO2/ZnO was prepared under ultrasonic irradiation by sol gel process from directly mixing Zirconium and Zinc gels, and the mixture was placed under ultrasonic irradiation for 2 hours then aging time the filtrated composite gel was calcinated at 500°C for 3h in furnace. The precursor sol of zirconium was prepared from an aqueous solution of ZrCl4 and zinc acetate dihydrated was...

Journal: :Nanoscale 2016
Samuel S Hinman Chih-Yuan Chen Jicheng Duan Quan Cheng

A patterned gold nanoparticle microarray, functionalized with a nanoscale silicate coating, has been developed for on-chip, high-throughput mass spectrometric analyses of biomolecules with minimal sample preparation and reagent costs. Fabrication was realized by the combination of layer-by-layer functionalization of the nanoparticles with suitable polyelectrolytes, followed by fluidic patternin...

A. Farhadyar M. Zare-Dehnavi N. Farhadyar Sh. Aghabeygi,

Nanocomposite of ZrO2/ZnO was prepared under ultrasonic irradiation by sol gel process from directly mixing Zirconium and Zinc gels, and the mixture was placed under ultrasonic irradiation for 2 hours then aging time the filtrated composite gel was calcinated at 500°C for 3h in furnace. The precursor sol of zirconium was prepared from an aqueous solution of ZrCl4 and zinc acetate dihydrated was...

The present study deals with analysis of the activity of catalysts prepared by addition of different metals to Copper and Cobalt based catalysts for CO oxidation and the variation in activity caused by changes in composition. A series of catalysts were prepared with Cu:Co molar ratio 1:4 and a third metal (M= Ce, Ni, Au, Mg) was added in three different quantities. Compositions were prepared by...

Nano hexagonal wurtzite ZnO has been prepared on zeoliteA by the sono-chemical method. The zeoliteA was mixed into Zinc gel, after stirring for two days, the mixture was irradiated 30 min by ultrasonic probe. The filtrated composite gel was calcinated at 500°C for 3h in furnace. The produced composite was characterized using X-ray diffraction, FT-IR spectroscopy and field emission scanning elec...

In this study, the synthesis, characterization and controlled release behavior of new Hollow Silica Nano particles (HSNPs) and Magnetic Silica Nano Particles (MSNPs) were studied. Magnetic Silica Nano particles (MSNPs), as drug delivery vehicles, were synthesized through the coating of Fe3O4 nano-crystals with silica layers. The HSNPs were obtained by removal of Fe3O4 templates with hydrochlori...

Journal: :Silicon 2021

A strategy for the synthesis of hybrid ordered mesoporous silica-carbon (Si/C) materials with moderate pore volume and surface area has been developed from pre-calcinated MCM carbon precursor Tectonagrandis (TG) dry leaves powder by direct loading method. The pre-activated (PAC) TG was prepared assistance sulphuric acid partial chemical activation controlled studies method indicate that PAC is ...

Journal: :Catalysts 2023

Porous cerium oxide (ceria) nanoparticles were prepared with and without manganese (Mn) by using the flash combustion technique. Samples different loadings (Ce/Mn ratio ranged from 100 to 10) a one-step process water only as solvent. Moreover, citric acid was utilized fuel in an aqueous medium, overall synthesis mixture dried at °C overnight then calcinated 550 for 3 h. The obtained final solid...

Journal: :Journal of the American Chemical Society 2002
Chika Nozaki Claus G Lugmair Alexis T Bell T Don Tilley

A new molecular precursor strategy has been used to prepare a series of single-site catalysts that possess isolated iron centers supported on mesoporous SBA-15 silica. The iron centers were introduced via grafting reactions of the tris(tert-butoxy)siloxy iron(III) complex Fe[OSi(O(t)Bu)(3)](3)(THF) with SBA-15 in dry hexane. This complex reacts cleanly with the hydroxyl groups of SBA-15 to elim...

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