We present the on-surface reduction of diepoxytetracenes to form genuine tetracene on Cu(111). The conversion is achieved by scanning tunneling microscopy (STM) tip-induced manipulation as well as thermal activation and is conclusively demonstrated by means of atomic force microscopy (AFM) with atomic resolution. We observe that the metallic surface plays an important role in the deoxygenation ...

We analyze the dynamics of an atomic force microscopy AFM cantilever oscillating in liquid at subnanometer amplitude in the presence of tip-sample interaction. We present AFM measurements of oscillatory solvation forces for octamethylcyclotetrasiloxane on highly oriented pyrolitic graphite and compare them to a harmonic oscillator model that incorporates the effect of the finite driving force f...

Atomic force microscopy (AFM) offers unparalleled insight into structure and material functionality across nanometer length scales. However, the spatial resolution afforded by the AFM tip is counterpoised by slow detection speeds compared to other common microscopy techniques (e.g., optical, scanning electron microscopy, etc.). In this work, we develop an ultrafast AFM imaging approach allowing...

Nanoscale characterization of living samples has become essential for modern biology. Atomic force microscopy (AFM) creates topological images of fragile biological structures from biomolecules to living cells in aqueous environments. However, correlating nanoscale structure to biological function of specific proteins can be challenging. To this end we have built and characterized a correlated ...

Lateral projections of neurofilaments (NF) called sidearms (SA) affect axon stability and caliber. SA phosphorylation is thought to modulate inter-NF distance and interactions between NF and other subcellular organelles. SA were probed by atomic force microscopy (AFM) and dynamic light scattering (DLS) as a function of phosphorylation and ATP content. DLS shows SA are larger when phosphorylated...

Visualisation of nano-scale biomolecules aids understanding and development in molecular biology and nanotechnology. Detailed structure of nucleosomes adsorbed to mica has been captured in the absence of chemical-anchoring techniques, demonstrating the usefulness of non-contact atomic force microscopy (NC-AFM) for ultra-high resolution biomolecular imaging. NC-AFM offers significant advantages ...

Langmuir monolayers of semi-fluorinated nonadecylphosphonic acid (F8H11PO3), hexadecylphosphonic acid (H16PO3), and their mixtures were investigated by Brewster angle microscopy (BAM), atomic force microscopy (AFM) and surface-pressure measurements. Nanometre-scale two-dimensional clusters were observed by AFM in a spread monolayer of pure F8H11PO3 transferred to mica. Two different organized a...

This paper has reported on the electrical and nonstructural of polymer-based materials in corporation NiO (Nickel oxide) in concentrations of 0.2%, 0.4% and 0.8% by weight of PVA (polyvinyl alcohol) polymer. Nanocrystallites phases and properties were characterized with using X-ray diffraction (XRD), Fourier transfer infrared radiation (FTIR),Energy distribution X-ray(EDX) techniques and X-Map ...

In this study, we present a new technique called correlative atomic force and transmission electron microscopy (correlative AFM/TEM) in which a targeted region of a sample can be observed under AFM and TEM. The ultimate goal of developing this new technique is to provide a technical platform to expand the fields of AFM application to complex biological systems such as cell extracts. Recent adva...