In this work, sol-gel processing was used to synthesize the fluorohydroxyapatite (nano-FHA, Ca10(PO4)6(OH)2−xFx) nanopowders. The advantages of the sol-gel method over other methods are precise control of composition, low processing temperature, and better homogeneity. Calcium nitrate tetrahydrate, phosphorous pentoxide and Tetrabuthylammon...

x-ray diffraction peak profile analysis was used to identify changes in the lattice distortions during isothermal aging of fe-10ni-7mn (wt. %) maraging steel. integral peak breadths were analyzed using classical williamson-hall equation taking the elastic anisotropy into account. it was found that substantial lattice distortions rise during precipitation hardening which depend strongly on the s...

In this study, the effects of mechanical milling and YSZ reinforcing on oxidation behavior of CoNiCrAlY coatings were investigated. Various amounts of YSZ particles (0%, 5%, 10% and 15 wt.%) were mixed with commercial CoNiCrAlY powder and milled for 24 hrs. Then, the mechanically milled and commercial powders were deposited on Inconel 617 substrate using High Velocity Oxygen-Fuel (HVOF) process...

A facile and environmentally friendly surface-ion adsorption method using CeCO₃OH@C as template was demonstrated to synthesize CeO₂-LaFeO₃ perovskite composite material. The obtained composite was characterized by X-ray diffraction (XRD), fourier transform infrared spectra (FT-IR), field-emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), thermo-gravimetric a...

A Synthesis of doped ceria by combustion method is performed. Two types of fuel such asurea and glycine is used to investigate the effect of fuel reactivity and reaction rate on themorphology of the resulted powders. Thermo gravimetric analysis is carried out by (TG/DTA,Rigaku Thermalplus TG 8120) to study the exo–endo temperature of as-received powder. Thecrystalline phases are identified by X...

Zirconia doped Hydroxyapatite (HAP) nanocrystals [Ca10(PO4)6-x(ZrO2)x(OH)2]; (0 ≤ x ≤ 1 step 0.2) were synthesized using simple low cost facile method. The crystalline phases were examined by X-ray diffraction (XRD). The crystallinity percentage decreased with increasing zirconia content for the as-synthesized samples. The existence of zirconia as secondary phase on the grain boundaries; as obs...

The ternary blends consisting of Chitosan (CS), Nylon6 (Ny6) and Polyurethane foam (PUF) were prepared by solution blending method. The Structural, thermal and morphological studies were performed by Fourier transform infrared spectroscopy (FTIR), Thermo gravimetric analysis (TGA), X-ray diffraction (XRD) and Scanning electron microscope (SEM). The FTIR results showed intermolecular hydrogen bo...

A new methodology is presented that allows the rapid determination of elastic constants of cubic fibre-textured thin films by X-ray diffraction. The theoretical concept is developed and tested on calculated examples of Cu and CrN films. The mechanical elastic constants are extrapolated from X-ray elastic constants by taking into consideration crystal and macroscopic elastic anisotropy. The deri...

Analysis of tomographic datasets at synchrotron light sources (including X-ray transmission tomography, X-ray fluorescence microscopy and X-ray diffraction tomography) is becoming progressively more challenging due to the increasing data acquisition rates that new technologies in X-ray sources and detectors enable. The next generation of synchrotron facilities that are currently under design or...