نتایج جستجو برای: spme gc ms

تعداد نتایج: 146198  

Journal: :Plant and Soil 2023

The colonization of plant growth-promoting rhizobacteria (PGPR) along roots in turn facilitates their ability to promote growth and health. In this study, we found that Bacillus subtilis strain WM13-24 from the rhizosphere Haloxylon ammodendron was able both Arabidopsis its host plant. Furthermore, volatile organic compounds (VOCs) could by stimulating lateral root formation hair growth. Howeve...

Journal: :Journal of chromatography. A 2014
Marie Marchini Céline Charvoz Laurence Dujourdy Nicolas Baldovini Jean-Jacques Filippi

The volatile constituents of drug samples derived from Cannabis sativa L. were investigated by means of headspace solid phase microextraction (HS-SPME) and gas chromatography techniques (GC-MS, GC×GC-MS). Samples of cannabis herb and hashish showed clear differences in their volatile chemical profiles, mostly resulting from photo-oxidation processes occurring during the transformation of fresh ...

2013
Celia Eliane de Lara da Silva Willian Ferreira da Costa Sandro Minguzzi Rogério Cesar de Lara da Silva Euclésio Simionatto

The chemical composition of essential oil and volatile obtained from the roots of Jatropha ribifolia (Pohl) Baill was performed in this work. The Clevenger extractor was utilized in hydrodistillation of oil and chemical composition determined by gas chromatography coupled with mass spectrometry detector (GC-MS). The identification of compounds was confirmed by retention index (Kovats index) obt...

2016
Stefano Gentili Renata Solimini Roberta Tittarelli Giulio Mannocchi Francesco Paolo Busardò

The reliability of DrugWipe 5A on site test for principal drugs of abuse (cannabis, amphetamines, cocaine, and opiates) detection in oral fluid was assessed by comparing the on-site results with headspace solid-phase microextraction (HS-SPME) gas chromatography-mass spectrometry (GC-MS) analysis on samples extracted by the device collection pad. Oral fluid samples were collected at recreational...

Journal: :Journal of agricultural and food chemistry 2014
António César Silva Ferreira Ana Rita Monforte Carla Silva Teixeira Rosa Martins Samantha Fairbairn Florian F Bauer

This work describes the utility and efficiency of a metabolic profiling pipeline that relies on an unsupervised and untargeted approach applied to a HS-SPME/GC-MS data. This noninvasive and high throughput methodology enables "real time" monitoring of the metabolic changes inherent to the biochemical dynamics of a perturbed complex biological system and the extraction of molecular candidates th...

Journal: :Journal of Food Quality 2021

A combined untargeted and targeted approach was established for fingerprinting volatile organic compounds in winter jujubes from eight regions of China. Volatiles, including alcohols, aldehydes, acids, esters, alkenes, were identified by gas chromatography-ion mobility spectrometry (GC-IMS). Benzyl alcohol, octanoic acid, 2-hexenal, linalool, 2-nonenal, ethyl decanoate the most common present a...

Journal: :Applied sciences 2023

In this paper, a new protocol is described, based on solid phase microextraction (SPME) coupled with gas chromatography–mass spectrometry (GC-MS), to monitor ex vivo changes in endogenous volatile organic compounds (VOCs) released by surgically resected colonic tissues (normal mucosa and adenomatous polyps) from seven patients undergoing operative colonoscopy identify their molecular pattern. T...

Journal: :Proceedings 2021

The aim of this article was the gas chromatography–mass spectrometry (GC-MS) analysis oforganic matter from a residual liquor sample (S.C. Alum S.A., Tulcea), extracted by solid-phasemicroextraction method (SPMA) and derivatized with N-(tert-butyldimethylsilyl)-Nmethyltrifluoroacetamide(MTBSTFA) as silylating agent. [...]

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