Smokeless powder additives are usually detected from an extraction of post-blast residues or unburned powder particles followed by chromatographic analyses. This work presents the first comprehensive study of the detection of volatile and semi-volatile additives of smokeless powders using solid phase microextraction (SPME) as a sampling and pre-concentration technique. The goal of this study is...

nanostructured ruo2 powders were synthesized via a hydrothermal method at 180 °c for 12 h using 1 and 2 m naoh aqueous solutions. the structure of the obtained nanomaterials was investigated by powder x-ray diffraction (pxrd) technique. the morphology the obtained materials were studied by field emission scanning electron microscope (fesem). the technique showed that with changing the reaction ...

Abstract The phase and structural changes of steel powders CL20ES CL50WS used in additive manufacturing were studied by Mössbauer spectroscopy X-ray diffraction. Investigated annealed the temperature range 500 °C–1100 °C oxidizing inert atmosphere. Annealing an atmosphere resulted formation different iron oxides both depending on annealing temperature. In addition, a change ferrite to austenite...

ZnFe2O4 yolk-shell powders were prepared by applying a simple spray-drying process. Dextrin was used as a drying additive and carbon source material, and thus played a key role in the preparation of the powders. The combustion of precursor powders consisting of zinc and iron salts and dextrin obtained by a spray-drying process produced the yolk-shell-structured ZnFe2O4 powders even at a low pos...

Nickel and aluminum powders were mechanically alloyed with 10 or 30 vol.% refractory metal powders (molybdenum or tungsten) for times up to 50 h. Intermetallic synthesis takes place after lo-20 h alloying, with concomitant dispersion of the inert refractory metal phase, resulting in an NiAl matrix containing fine refractory dispersoids. The reactive synthesis step is direct, without intermediat...

We prepared various types of yuja powders from juice, fruit, and seed (to maintain the unique flavor) by using different homogenization drying methods investigated their physicochemical properties. To this end, ultrasonic high-pressure homogenization, were carried out to obtain mixtures. These mixtures subjected via spray-drying, freeze-drying, microwave vacuum-drying spray-dried, freeze-dried,...

203Hg, 35S or 131I labeled mercury (II) iodide thiocyanate (HgISCN) powders were prepared, respectively. When the powders were exposed to sunlight, some parts of the crystals of the powders were decomposed and the decomposed atoms diffused toward crystal surface. This diffusion velocity was accelerated by thermal treatment of the darkened powders. The velocity is larger in order of 35S, 203Hg, ...

Nanostructured Mn2Sb2O7 powders were synthesized via stoichiometric1:1 Mn:Sb molar ratio solid state reaction at different reactions temperatures for 8 h using MnSO4.H2O and Sb2O3 as raw materials. The synthesized materials were characterized by powder X-ray diffraction (PXRD) technique. Structural analyses were performed by the FullProf program employing profile matching with constant scale fa...