نتایج جستجو برای: sol gel method and xrd technique
تعداد نتایج: 17121661 فیلتر نتایج به سال:
tourism , today as one of the ways to make money, create jobs , and social and political interactions is considered. this paper aims to examine the strengths and weaknesses of tourism development in mahmoud abad ( mazandaran ). the research method in this study is " descriptive - analytical " and to collection of data used field methods such as questionnaires and documentation - library. the sa...
preparation and characterization of thermoresponsive in-situ forming poloxamer hydrogel for controlled release of nile red-loaded solid lipid nanoparticles. nanoparticles (nps) are cleared rapidly from systemic circulation and do not provide sustained action in most cases. to solve this problem, this investigation introduces an erodible in-situ forming gel system as potential vehicles for prolo...
In this research, a sol-modified composite electrodeposition technique that combines the sol-gel method with the conventional electrodeposition process was utilized to deposit Ni-TiO2 nanocomposite coatings. Cyclic voltammetry and chronoamperometry techniques were applied to study the influence of the TiO2 sol concentration on the deposits’ electrochemical behavior. The results clearly showed t...
The highly efficient Vanadium doped ZnO nano-rod supported with MWCNT (V@ZnO/MWCNT) has been fabricated using a convenient sol-gel impregnation method. techniques such as FTIR, XRD, UV-Vis DRS, TEM, and...
Hybrid sols of poly (vinyl alcohol) (PVA)/Silicon oxide-titanium oxide (SiO2-TiO2) were prepared with tetraethoxylsilane and tetrabutyl titanate as precursor using Sol-Gel method. PVA/SiO2-TiO2 hybrid fibers were prepared by drawing from the hybrid sols using dip-coating method and aging treatment. The spinnability of hybrid sols was investigated. Spinnable time (t) and spinnable length (l) of ...
In this paper, indium tin oxide (ITO) nanoparticles has been prepared by chemical methods under given conditions with solution of indium chloride (InCl3·4H2O), tin chloride (SnCl4·5H2O) in ammonia solution. The samples were characterized by X-ray Diffraction (XRD) and scanning electron microscopy (SEM) analyses after heat treatments. The SEM results showed that, the size of the ITO particles pr...
Nanocrystalline thin film of Na0.1V2O5.nH2O xerogel obtained by sol gel synthesis was used as gas sensor. Gas sensing properties of different gases such as hydrogen, petroleum and humidity were investigated. Applying XRD and TEM the size of the nanocrystals is found to be 7.5 nm. SEM shows a highly porous structure with submicron meter-sized voids present throughout the sample. FTIR measurement...
Nano ZnO/ montmorillonite composite were prepared by sol gel method under ultrasonic irradiation from directly mixing montmorillonite nano clay into Zinc gel. The Zn(CH3COO)2.2H2O and montmorillonite nano clay was used as precursor. The zinc acetate was dissolved in DI water and, NH3 (aq) solution was dropped into the zinc solution until pH 9 consequently the zinc gel was produced. The montmori...
Hydroxyapatite (HAP) ceramics belongs to a class of calcium phosphate-based biomaterial, which has been widely used as bone substitute for long time. In recent years, synthetic HAP has assumed substantial interest and importance due to its chemical similarity with the natural Ca phosphate mineral present in a biological hard tissue. Considering the wide applications of calcium phosphate compoun...
This article describes the preparation and analysis of nano hydroxyapatite (HA) films on stainless steel 316L through sol-gel technique. The process started with preparation of a nitrate and phosphate sol. After aging the sol for 24 h at room temperature a SS316 substrate was dip-coated and heat-treated at 350 to 450 °C for different times in air. The coating phase and structure on subs...
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