the synthesis of titania via sol-gel method has been widely studied. in the present work, titania was deposited onto a titanium substrate via sol-gel method. different processing parameters such as the repetition number of dipping/heat treatment process and dipping time have been studied to obtain the homogenous titania coating. phase and microstructural evaluation of the powder and coating sam...

Silica aerogels are among the most easily produced types of aerogels due to the availability of required materials, the cheapness of required materials such as carbon dioxide, ethanol, and tetraethyl orthosilicate, and the relatively simple sol-gel chemistry. Using silica aerogels as skeletons, nanomaterials were easily and effectively structured in three dimensions. The aerogels were doped wit...

Mesoporous α-Fe2O3 thin films with large area homogeneity demonstrate tremendous potential in multiple applications. In the present work, synthesis of morphology-controlled is realized polystyrene-block-poly(4-vinyl pyridine) (PS-b-P4VP) diblock copolymer assisted sol-gel chemistry. The solvent category (DMF and 1,4-dioxane) polymer-to-FeCl3 ratio used for solution preparation are systematicall...

Spectrally resolved infrared stimulated vibrational echo spectroscopy is used to measure the fast dynamics of heme-bound CO in carbonmonoxy-myoglobin (MbCO) and -hemoglobin (HbCO) embedded in silica sol-gel glasses. On the time scale of approximately 100 fs to several picoseconds, the vibrational dephasing of the heme-bound CO is measurably slower for both MbCO and HbCO relative to that of aque...

cotio3-clay nano-composites were synthesized via a conventional sol-gel method; the gel was calcinated at 500 - 800°c for 2 hours. the presence of rhombohedra phase of cotio3 in clay matrix was confirmed by xrd, ftir, sem. cobalt titanate-clay nano-composites were prepared with 5-20%(w/w) by sol-gel method. the spectra results were investigated at 20% (w/w) concentration .the optimum condition ...

in this research fe-tio2 nanocomposites with different molar ratios of fe/ti were prepared as nano-photocatalyst using a modified sol-gel process at ambient temperature. crystallographic properties of nanocomposites were characterized by x-ray diffraction (xrd). surface morphology and mean particle size of nanocomposites were specified by field emission scanning electron microscopy (fesem) and ...

in recent years, using sol-gel procedure for the purpose of laboratory and industrial synthesis of nano-structures, and especially silica nano-particles, has been significantly increased. in this research, silica particles were synthesized by sol-gel procedure and their physical and chemical properties were studied by means of scanning electron microscopy (sem), transmission electron microscopy...

in this work firstly zno nanoparticles were synthesized via a simple precipitation method. at the second step titanium dioxide and silicon dioxide shell were synthesized on the core. for preparation zno-tio2-sio2 the sol product was calcinated at 500 ºc for 2h. properties of the product were examined by x-raydiffraction pattern (xrd), scanning electron microscope (sem) and fourier transform inf...

the stabilized zirconia with different cu contents synthesized via sol-gel method. the samples were prepared by hydrolysis and condensation of orgnomatelic sol. after that the result gels were dried at 80 °c and then calcined at various temperatures.  ِ the differential thermal analysis (dta), x-ray diffraction (xrd), field emission scanning electronic microscopy (fesem) and transmission electro...