a simple and rapid microextraction procedure based on dispersive liquid-liquid microextraction (dllme) coupled with gas chromatography-flame ionization detection (gc-fid) was developed for the extraction and analysis of 2-phenylethanol in rose water sample. in the proposed approach, carbon tetrachloride and ethanol were used as extraction and dispersive solvents, respectively. some important pa...

the effects and influences of various parameters upon the efficiency and the overall volumetric mass transfer coefficients are important subjects to be studied in most liquid-liquid extraction processes. one of these important parameters is surface active agent (surfactant). in this paper, in order to study the effect of sodium dodecyl sulfate (sds) concentration on the efficiency and the avera...

background & aim: according to the increase in diseases such as diabetes and obesity, using of saccharose alternatives for producing of low-calorie and sugar-free alternatives, are taken into consideration of researchers and industrialists. among them, steviosidewith the 300 times more sweetness than saccharose has special place, due to is a natural. the aim of this study is optimizing of stevi...

A simple and rapid microextraction procedure based on dispersive liquid-liquid microextraction (DLLME) coupled with gas chromatography-flame ionization detection (GC-FID) was developed for the extraction and analysis of 2-phenylethanol in rose water sample. In the proposed approach, carbon tetrachloride and ethanol were used as extraction and dispersive solvents, respectively. Some important pa...

An effective ionic liquid vacuum microwave-assisted method was developed for extraction of the thermo- and oxygen-sensitive glycosides salicin, hyperin and rutin from Populus bark due to the strong solvating effects of ionic liquids on plant cell walls. In this study, [C4mim]BF4 solution was selected as the extracting solution for extraction of the target analytes. After optimization by single ...

In this paper, microwave-assisted extraction (MAE) of oxymatrine from Sophora flavescens were studied by HPLC-photodiode array detection. Effects of several experimental parameters, such as concentration of extraction solvent, ratio of liquid to material, microwave power, extraction temperature, and extraction time on the extraction efficiencies of oxymatrine were evaluated. The optimal extract...

phenolic compounds, especially those of plant origin, constitute an essential part of the human diet, and are of considerable interest due to their antioxidant properties. in this study, ultrasound-assisted extraction (uae), microwave-assisted extraction (mae), as well as maceration extraction (me) methods were applied for phenolic compounds’ extraction from pistachio green hull. response surfa...

A simple, inexpensive and sensitive three-phase hollow fiber liquid-phase microextraction (HFLPME) coupled with high performance liquid chromatography (HPLC) with UV detection was successfully developed for determination of trace level of an anti-Histamine drug, fexofenadine, in human plasma and urine. The analyte was extracted into n-octanol that was immobilized in the wall of a porous hollow ...

Process engineers can be faced with the task of understanding and optimizing the performance of an existing liquid-liquid extraction (extraction) column. Often times, an extraction column has been operating many years, and the performance is not well understood by the personnel responsible for its operation. Since this technology is not treated comprehensively during most under-graduate Chemica...

The objective of the study was to optimize the processing of Microwave-Assisted Extraction (MAE) of flavonoids from Cryptotaenia japonica Hassk. The effects of processing parameters include ethanol proportion, extraction time, extraction temperature and ratio of liquid to solid on the flavonoids yield were determined and the optimal conditions for flavonoids were evaluated by means of Response ...