the brønsted acidic ionic liquid ([bmim]hso4) catalyzed three-component synthesis of 2h-indazolo[2,1-b]phthalazine-trione derivatives at room temperature. the integrity of the ionic liquid remains reasonably unchanged when it is separated from the reaction mixture by water extraction, as it can be recycled several times without any loss of activity in each of the title syntheses. the products a...

microwave assisted green synthesis of α, ά- bis (substituted- benzylidene) alkanones by the crossed- aldol condensation reaction of substituted aryl aldehydes with ketones in the presence of catalytic amount of nbcl5 in good to excellent yields. this reaction is carried out under solvent-free conditions. the results showed that aldehydes bearing electron–donating substituent's on phenyl-ring fa...

A new kind of data model has recently emerged in which the database is not constrained by a conventional schema. Systems like ACeDB, which has become very popular with biologists, and the recent Tsimmis proposal for data integration organize data in tree-like structures whose components can be used equally well to represent sets and tuples. Such structures allow great exibility in data represen...

 phenytoine derivatives were synthesized , via the  pinacol condensation  with the  reaction of 1,3- diphenyl- propane- 1,3- dione (benzyl) analogs with urea or thiourea in presence of slica gel and solid KOH as Solid phase catalyst  in the mortar / pestle at room temperatures. The reaction was completed at short reaction times (approximately 15min) and pure products were obtained with high yie...

Trichloroacetic Acid (TCA) was used as an efficient catalyst for the synthesis of highly functionalized piperidines via a one-pot five-component reaction of aromatic amines, aromatic aldehydes and β-keto esters in MeOH at room temperature. The remarkable advantages offered by this method are good yields, simple procedure, short reaction times, no need to column chromatography and an easy wo...

In this research, different alcohols and phenols are subjected to the reaction with HMDS in the presence of ionic liquid and silica-supported catalysts. Silylation was accomplished under mild reaction conditions at room temperature in short reaction times and good to excellent yields.

the substances responsible for saffron’s characteristic quality are crocins, picrocrocin, and safranal. the drying process is critical to the saffron quality as measured by levels of secondary metabolites, crocin (color and anti-tumor properties), picrocrocin (taste), and safranal (aroma). four different dehydration methods were evaluated: iranian traditional method (room temperature); dehydrat...

Prediction of interior room layout from observations on the exterior boundaries a unit is sometimes needed in cases emergencies when entry denied. Seeing that 3D laser scanners are becoming smaller, lighter, and easier to carry around, this paper attempts offer fast method can automatically reconstruct model relying merely point cloud boundaries. The first partitions building floor space genera...

Bed bugs, Cimex lectularius L., hide in cracks and crevices in furniture and are difficult to control. The bed bug thermal death kinetics were examined to develop a heat treatment method to eliminate bed bug infestations in room contents. High temperatures caused temporary immobilization (knockdown) of bed bugs even with exposures that did not have lethal effects. Exposure of bed bug adults to ...