polyvinylpyrrolidone  /  nickel  oxide  (pvp/nio)  dielectrics  were fabricated  with  sol-gel  method  using  0.2  g  of  pvp  at  different working  temperatures  of  80,  150  and  200  ºc.  structural  properties and surface morphology of the hybrid films were investigated by x-ray  diffraction  (xrd)  and  scanning  electron microscope  (sem) respectively. energy dispersive x-ray spectrosc...

Three high-silica mordenite zeolites differing in SiO440, ratio were prepared by direct synthesis without using any template. The products Si02/A120, ratio is influenced by the starting gel composition. This ratio is increased upon ion-exchange with NH,Cl and subsequent calcination to prepare protonic mordenite. The protonic mordenites with Si02/A1203ra tios of 14.6,29.2 and 34.6 were chara...

In this research we report synthesis of new Barium- Cobalt precursor complex with 2,6- pyridine dicarboxylic acid (dipic).Thecomplex[Ba(H2O)6][Co(dipic)2[(1)has been characterized using spectral methods (FT-IR, UV–Vis),elemental analysis and Cyclic voltammetric (CV) method. Also in this study we report thermal decomposition of inorganic precursor complex of (1).Characterization of the binary ox...

introduction: the aim of this study was to compare the chemical compounds of white proroot mineral trioxide aggregate (wmta) hydrated at different ph environments. methods and materials: mixed samples of wmta were kept in acidic (ph=5.4), neutral (ph=7.4) and alkaline (ph=9.4) environments for 48 h. then, x-ray diffraction (xrd) analysis was performed for both hydrated and powder forms of wmta....

Oxide nanoparticles can exhibit unique physical and chemical properties due to their limited size and a high density of corner or edge surface sites. In this study, MgO nanoparticle was synthesized using Mg(CH3COO)2 and hexamethylenetetramine as starting materials. The structure and optical properties of these particles are investigated by using X-ray diffraction (XRD), sc...

in this paper, nano fibers (engelhard corporation titanosilicate number 10 / polyacrylonitrile) ets-10 / pan, as a composite exchanger to absorb heavy metals, were synthesized and optimized. several parameters were affected on this absorption. results show that the optimization sizes of the nano fibers are about 75 nanometers. structures were analyzed by scanning electron microscope (sem) and e...

An X-ray diffraction line will broaden considerably when steels change into martensitic structure on quenching. The results presented in this paper show that X-ray diffraction technique can be employed for a rapid and nondestructive measurement of hardness of hardened steel. Measurement on various quenched and tempered steels showed that the breadth of its diffraction peak increased with increa...

X-ray diffraction peak profile analysis was used to identify changes in the lattice distortions during isothermal aging of Fe-10Ni-7Mn (wt. %) maraging steel. Integral peak breadths were analyzed using classical Williamson-Hall equation taking the elastic anisotropy into account. It was found that substantial lattice distortions rise during precipitation hardening which depend strongly on the s...

Background: Proton induced X-ray emission (PIXE) has been applied as reliable and improved techniques in this study to compare concentration of various trace elements in normal and abnormal varicose veins. Materials and Methods: Five samples from normal veins and 13 samples from varicose veins bombarded by 2.0 MeV energy proton beams produced by a Van de Graff accelerator in vacuum. T...