The ultrasound-assisted (UA) soybean oil methanolysis using KOH as a catalyst was studied at different reaction conditions in a microreactor. Box–Behnken experimental design, with three variables, was performed and the effects of three reaction variables i.e. reaction temperature, catalyst concentration and the methanol-to-oil molar ratio on fatty acid methyl ester (FAME) yield were evaluated b...

In this work we investigate the effect of iron oxide embedded in silica matrices as a function of Fe/Si molar ratio and sol pH. To achieve homogeneous dispersion of iron oxide particles, iron nitrate nonahydrate was dissolved in hydrogen peroxide and was mixed with tetraethyl orthosilicate and ethanol in a sol-gel synthesis method. Increasing the calcination temperature led to a reduction in su...

The extent of poly -caprolactone (PCL) incorporation into silica networks prepared by the sol-gel process depends on the HCl:tetraethoxysilane (TEOS) molar ratio and the H2O:TEOS molar ratio, as well. The PCL incorporation increases with the concentration of the acid used as the catalyst. Dynamic mechanical analysis (DMA) indicates that increasing the acid concentration or decreasing the water ...

nanocrystalline particles of cerium oxide (ceo2) have been prepared by the chemical precipitation method using cerium nitrate and urea with a molar ratio of 1:2. the results revealed that the formation of ceo2 fine particles is influenced by molar ratio of metal nitrates to fuel. well faceted ceo2 nanoparticles, were synthesized by thermal-assisted dissociation method at reflux temperature in a...