نتایج جستجو برای: microwave assisted

تعداد نتایج: 176049  

Glycerol mono-oleate (GMO) was produced by direct esterification reaction with amberlyst 16 resin catalysts with the efficiency of 86% and was used as a surfactant for synthesis of CoFe2O4 nano-particles by surfactant-assisted microwave method. Fourier transform infrared spectroscopy (FT-IR), X-Ray diffraction (XRD) and scanning electron microscopy (SEM) were used to consider the structural and...

2010
B Mistry Dipti Medhane Krishnapriya Mohanraj Sanjeevani A. Ghone

Rapid and efficient methods for the synthesis of an important intermediate of benazepril ethyl 3-phthalimido-2,3,4,5-tetrahydro-1H-[1]benzazepin-2-one-1-acetate under the influence of microwave irradiation are described. A comparative study of conventional and microwave assisted method is briefly discussed.

2014
Alexey P. Slobozhanyuk Irina V. Melchakova Constantin R. Simovski Pavel A. Belov

Articles you may be interested in Microwave absorptions of ultrathin conductive films and designs of frequency-independent ultrathin absorbers Influence of lattice parameters on the resonance frequencies of a cut-wire-pair medium Experimental study of surface-wave-assisted microwave transmission through a single subwavelength slit

2000
S. Kataoka D. T. Tompkins M. A. Anderson M. E. Zorn W. A. Zeltner J. H. Booske

Photocatalytic oxidation makes use of light of appropriate frequency to activate a catalyst. In the presence of water on the surface of the catalyst, rates of some photocatalytic reactions are slowed. Microwaves are known for an ability to couple with water. Herein a photocatalytic reactor system was integrated with a waveguide allowing for concurrent application of microwaves and photocatalysi...

2012
Angeles Cancela Santiago Urrejola Angel Sanchez

Nowadays microwave radiation is being researched to produce biodiesel from different raw materials due to the many advantages that this technology presents compared to traditional transesterification, such as shorter reaction times and less amount of heat energy to obtain biodiesel. The aim of this research was to explore the possibility of carrying out the microwave-assisted transesterificatio...

Journal: :The Journal of organic chemistry 2005
Andreas Svennebring Neeraj Garg Peter Nilsson Anders Hallberg Mats Larhed

A fast one-pot method has been developed for the direct preparation of 3-aryl-1,2-cyclohexanediones from 2,3-epoxycyclohexanone via a microwave-assisted tandem epoxy ketone isomerization-Heck arylation reaction. The preparative microwave-assisted reactions were performed preferentially in 50% aqueous poly(ethylene glycol) utilizing sodium acetate as the base. Within 5-30 min of directed microwa...

Journal: :Molecules 2010
Monica Gallo Rosalia Ferracane Giulia Graziani Alberto Ritieni Vincenzo Fogliano

Spices and herbs are known not only for their taste, aroma and flavour, but also for their medical properties and value. Both spices and herbs have been used for centuries in traditional medical systems to cure various kinds of illnesses such as common cold, diabetes, cough and cancers. The aim of this work was the comparison between two different extractive techniques in order to get qualitati...

Journal: :Analytical chemistry 2007
Wei-Yu Chen Yu-Chie Chen

The presence of alkali cation adductions of oligonucleotides commonly deteriorates matrix-assisted laser desorption/ionization (MALDI) mass spectra. Thus, desalting is required for oligonucleotide samples prior to MALDI MS analysis in order to prevent the mass spectra from developing poor quality. In this paper, we demonstrate a new approach to extract traces of oligonucleotides from aqueous so...

Glycerol mono-oleate (GMO) was produced by direct esterification reaction with amberlyst 16 resin catalysts with the efficiency of 86% and was used as a surfactant for synthesis of CoFe2O4 nano-particles by surfactant-assisted microwave method. Fourier transform infrared spectroscopy (FT-IR), X-Ray diffraction (XRD) and scanning electron microscopy (SEM) were used to consider the structural and...

2013
Hemanth Mohandas Gunalan Sivakumar Palaniappan Kasi Saravana Kumar Jaganathan Eko Supriyanto

A wide number of polymers are being used for various medical applications. In this work, microwave-assisted surface modification of metallocene polyethylene (mPE) was studied. FTIR analysis showed no significant changes in the chemical groups after treatment. Contact angle analysis revealed a decrease in contact angle of the treated samples insinuating increasing hydrophilicity and better bioco...

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