A new carboxylic acid extractant, named 2-(dibutylcarbamoyl)benzoic acid, is prepared and its potential for selective solvent extraction and recovery of lead ions from industrial samples was investigated. The slope analysis indicated that the lead ions are extracted by formation of 1:2 metal to ligand complexes. The effect of the parameters influencing the extraction efficiency including kind o...

a simple and rapid microextraction procedure based on dispersive liquid-liquid microextraction (dllme) coupled with gas chromatography-flame ionization detection (gc-fid) was developed for the extraction and analysis of 2-phenylethanol in rose water sample. in the proposed approach, carbon tetrachloride and ethanol were used as extraction and dispersive solvents, respectively. some important pa...

Background and Objectives: Supercritical fluid extraction (SFE) technique has been studied for extraction of bioactive compounds from Feijoa sellowiana leaves. Results were compared with those obtained from conventional ethanolic extraction (CE). Materials and Methods: Results: The best supercritical carbon dioxide (SC-CO2) extraction conditions was determined as 250 bar of pressure, 50 &deg...

This work was initiated to study the concentration effects on phenanthrene and pyrene extraction during process of aging in phaeozem and burozem with or without freeze-thawing cycles. 1, 10, and 100 μg g(-1) phenanthrene and pyrene contaminated soils were extracted by 10,000 mg L(-1) surfactant SDBS at various times. The extraction amount decreased with increasing contact time. Aging process co...

Purpose: To develop a more green, efficient and low cost process for the extraction of steroidal saponins from Dioscorea Zingiberensis C. H. Wright. Methods: Six kinds of ionic liquids with different cations and anions were evaluated. In addition, the extraction parameters of the ionic liquid based ultrasonic/microwave extraction were studied. In order to quantify the total saponin content accu...

The electrochemical coating technique was used for the preparation of a polypyrrole coating on a stainless-steel wire, and applied as a fibre for solid phase microextraction (SPME). The polypyrrole fibre was employed for analyzing four volatile aliphatic amines (ethylamine, propylamine, butylamine and pentylamine) in water by headspace SPME using gas chromatography-flame ionization detection (G...

Background & Aim: Sesame is one of the oldest cultivated plants in the world and is one of the oldest oily products used by humans. Sesame oil is an important industrial, oral and medicinal oil. Today, the use of ultrasound has grown significantly due to its effects on food storage and processing. Experimental: In this research, the response level model w...

abstract: aqueous enzymatic extraction of oil from pistacia khinjuk was performed using cellulase. the central composite design was used to optimize the parameters that are significant to the process. the influence of three regressors on the percentage of oil recovery from seed was evaluated using second-order polynomial multiple regression model. analysis of variance showed a high coefficient ...

agar is a gelling biopolymer that can be extracted from cell wall of some red algae. in this present, response surface methodology was used to investigate the procedure of agar melting point and gelling temperature from cultural algae of gracilariopsis persica. independent variables, alkalinity concentration (2, 3.2, 5, 6.8, -8%), extraction temperature (90, 96, 105, 114, 120°c) and extraction ...

A simple, rapid, and ultra sensitive dispersive solid phase extraction based on nano graphene oxide was developed for simultaneous measurement of trace amounts of metformin (MET) and linagliptin (LIN) in plasma samples by HPLC-UV-Vis. Affecting factors on the extraction of these drugs, including adsorbent weight, extraction time, organic solvent type, desorption situations, and composition of s...