in this study, the tio2 nanorods were synthesized from p25 tio2 nanoparticles by hydrothermal method in 10 m naoh solution. the effects of annealing temperatures on produced nanorods were investigated  by scanning  electron microscopy (sem) x-ray diffraction (xrd) and photoluminescence (pl) spectroscopy. diameter growth and  changes  of  surface  oxygen  defects of  synthesized nanorods are stu...

in this paper, cuo nanoparticles  have been synthesized via solid-state thermal decomposition using copper(ii) schiff base complexes as new precursors at 600ºc under air atmosphere for 3 h. surface morphology of the products were characterized by fourier transform infrared spectroscopy (ft-ir), x-ray diffraction (xrd) and scanning electron microscopy (sem).

Electron microscopy of materials in a gaseous environment has its origins as far back as about the 1950s for the transmission electron microscope (TEM), later followed by developments for the scanning electron microscope (SEM). Focusing on the latter, this review outlines the history and commercial development of the technology, culminating in the environmental SEM (ESEM), and the techniques fo...

iron oxide (fe2o3) nanoparticles were synthesized by a simple approach using sodium borohydride (nabh4) and iron chloride hexahydrate (fecl3.6h2o). their physicochemical properties were characterized by high resolution transmission electron microscopy (hrtem), scanning electron microscopy (sem), x-ray diffraction (xrd) and electron dispersive spectroscopy (eds). xrd pattern showed that the iron...

The FIB/SEM system was satisfactorily used for scanning ion (SIM) and scanning electron microscopy (SEM) of gland epithelial cells of a terrestrial isopod Porcellio scaber (Isopoda, Crustacea). The interior of cells was exposed by site-specific in situ focused ion beam (FIB) milling. Scanning ion (SI) imaging was an adequate substitution for scanning electron (SE) imaging when charging rendered...

Testate amoebae (TA) are a group of free-living protozoa, important in ecology and paleoecology. Testate amoebae taxonomy is mainly based on the morphological features of the shell, as examined by means of light microscopy or (environmental) scanning electron microscopy (SEM/ESEM). We explored the potential applications of confocal laser scanning microscopy (CLSM), two photon excitation microsc...

Microscopical tests, including polarized light microscopy (PLM), phase contrast microscopy (PCM), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were used along with X-ray diffraction (XRD) in the characterization and testing of a laboratory-grade “Gooch fiber” asbestos sample. The sample was tested for possible fiber release during typical use as a substrate for ...

The availability of two-dimensional (2-D) dopant profiling techniques to Silicon Carbide (SiC) pn junction is discussed. We compared the results of scanning capacitance microscopy (SCM), scanning spreading resistance microscopy (SSRM), and secondary electron microscopy (SEM), where the cross-sections of a SiC wafer with n-type epi-layers and highly-doped p and n regions were used. The SSRM curr...

introduction: successful endodontic treatment depends on elimination of the microorganisms through chemomechanical debridement. the aim of this in vitro study was to evaluate the effectiveness of fragaria vesca (wild strawberry) extract (fve) on the removal of smear layer (sl). methods and materials: in this analytical-observational study, 40 extracted mandibular and maxillary human teeth were ...

introduction: this study compared the cleaning efficiency of mtwo, race and medin nickel-titanium (niti) rotary instruments. materials and methods: sixty mandibular molar mesial roots were selected with angle curvatures between 25-35 degrees and divided into three groups; each containing 20 teeth. canals were prepared with the rotary files and irrigated with 2.5% naocl solution after each instr...