The electron microprobe allows elemental abundances to be mapped at the microm scale, but until now high resolution mapping of light elements has been challenging. Modifications of electron microprobe procedure permit fine-scale mapping of carbon. When applied to permineralized fossils, this technique allows simultaneous mapping of organic material, major matrix-forming elements, and trace elem...

A method of clay mineral sample preparation for electron microprobe analysis has been developed in which a film of clay plus 10-12 wt. % colloidal graphite is deposited on a porous ceramic disc using a specially designed suction device. Correction procedures are used to obtain quantitative elemental analyses representing the average chemical composition of the prepared sample. A statistical tec...

-A method of clay mineral sample preparation for electron microprobe analysis has been developed in which a film of clay plus 10-12 wt. % colloidal graphite is deposited on a porous ceramic disc using a specially designed suction device. Correction procedures are used to obtain quantitative elemental analyses representing the average chemical composition of the prepared sample. A statistical te...

Several of the fourteen rare-earth element (plus Sc and Y) orthophosphate standards grown at Oak Ridge National Laboratory in the 1980s and widely distributed by the Smithsonian Institution's Department of Mineral Sciences, are significantly contaminated by Pb. The origin of this impurity is the Pb2P2O7 flux that is derived from the thermal decomposition of PbHPO4. The lead pyrophosphate flux i...

Imaging the morphology of the tissue in vivo and producing the correspondent elemental maps, whether in major, minor, or trace concentrations in real-time can be done using a focused beam of accelerated particles. This can be accomplished using different ion beam techniques simultaneously such as Scanning transmission ion microscopy (STIM), secondary electron imaging (SEI), Rutherford backscatt...