نتایج جستجو برای: dta tga

تعداد نتایج: 8405  

Journal: :Politeknik dergisi 2021

In this study, synthesis and characterization of polymer/clay based nanocomposites was performed using 2-(4-methoxyphenyl amino)-2-oxoethyl methacrylate (MPAEMA) organoclay. The amount organoclay in synthesized by situ polymerization method determined as 3% 5%. FTIR, XRD, SEM were used techniques. It from XRD results that the morphology exfoliated. Then, thermal properties investigated TGA/DTA/...

M. Rafizadeh

A new metal-organic compound, [Fe(Pydc)(DMSO)(H2O)Cl], (where Pydc is pyridine-2, 6-dicarboxylate and DMSO is dimethyl sulfoxide), has been synthesized and characterized by singlecrystal X-ray diffraction, TGA/DTA, IR and Raman spectroscopy. Green-yellow crystals,crystallized in the monoclinic system, space group P21/n, a = 7.2461(4) Å, b = 10.3018(4) Å, c =17.7667(10) Å, α = 90°, β = 90.014°(5...

In this study, magnetite (Fe3O4) nanoparticles were synthesized by chemical co-precipitation from the solution containing iron salts in alkaline medium under N2 gas and room temperature. Magnetite nanoparticles were characterized by X- ray diffraction (XRD), Fourier transform infrared spectrometer (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), thermal gravim...

Journal: :Polycyclic Aromatic Compounds 2022

A highly efficient one-pot three-component protocol was devised for the synthesis of novel derivatives ((phenylethlidene)hydrazinyl)thiazol-4(5H)one by reaction acetophenone derivatives, ethyl chloroacetate and thiosemicarbazide, in ethanol at room temperature presence copper supported hydroxyapatite-encapsulated-γ-Fe2O3 (γ-Fe2O3@HAp@CPTMS@AT@Cu(ӀI)) as new magnetically recyclable heterogeneous...

Journal: :International journal of advanced academic studies 2021

In this research, Li1.25Mn0.125Ni0.125Co0.5O2 Nano powders, were synthesized using sol-gel method at different temperatures, lithium nitrate, manganese nickel cobalt nitrate as raw materials. Thermal and thermal gravimetric of TGA/DTA, characterization structure properties samples prepared by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) performed. Also, with scheme, i...

ژورنال: شیمی کاربردی 2013
حسین میقانی دباسیس داس علی اکبر دهنوخلجی, میلاد کاظم نژادی

در این مقاله، پلی‌سالیسیل آلدهید (PSA) بوسیله اکسایش تراکمی (OP) ترکیب ((2،4- دی کلروفنیل‌ایمینو) متیل) فنول با NaOCl و در محلول مایی نمک قلیایی بین دمای50 تا 90 درجه سلسیوس تهیه و به کمک تکنیک‌های 1H-NMR، FT-IR، UV-Visو TGA/DTA شناسایی شد. بازده تبدیل در شرایط بهینه [sal-2,4-Clan]0 = 0.02، [KOH]0= 0.1 و [NaOCl]0 = 0.12 mol/L، در دمای 90 درجه سلسیوس و مدت زمان 10 ساعت، 61.23% می‌باشد. بعلاوه، س...

Journal: :International journal of clinical and experimental medicine 2013
Doron Amit Sagi Tamir Abraham Hochberg

BACKGROUND The human IGF2-P4 and IGF2-P3 promoters are highly active in a variety of human cancers, while existing at a nearly undetectable level in the surrounding normal tissue. Thus, a double promoter DTA-expressing vector was created, carrying on a single construct two separate genes expressing the diphtheria toxin a-fragment (DTA), from two different regulatory sequences, selected from the...

Journal: :Cellular microbiology 2011
Lydia Dmochewitz Maren Lillich Eva Kaiser Laura D Jennings Alexander E Lang Johannes Buchner Gunter Fischer Klaus Aktories R John Collier Holger Barth

Bacillus anthracis lethal toxin consists of the protective antigen (PA) and the metalloprotease lethal factor (LF). During cellular uptake PA forms pores in membranes of endosomes, and unfolded LF translocates through the pores into the cytosol. We have investigated whether host cell chaperones facilitate translocation of LF and the fusion protein LF(N)DTA. LF(N) mediates uptake of LF(N)DTA int...

1999
Alexander K. Schomig

Discrete{time analysis (DTA) is a modelling technique that is mainly applied to the analysis of communication systems. In this paper, we show how DTA can be adopted to the numerical analysis of manufacturing systems. The modelling concepts of DTA are introduced and the advantages of DTA over other methods like discrete{event simulation are indicated. We apply DTA to two sample applications, nam...

This paper presents a systematic study of the surface chemistry, porous texture and adsorptive characteristics of prepared new activated carbon using Persian mesquite grain. Several techniques and methodologies such as, proximate analysis, N2 adsorption–desorption isotherms, scanning electron microscope (SEM), Fourier transform infrared spectroscopy(FT-IR), X-ray Diffraction (XRD), X-ray photoe...

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