نتایج جستجو برای: differential scanning calorimetry dsc

تعداد نتایج: 444301  

2013
Jhalique Jane R. Fojas Rizalinda L. De Leon

The characterization of κ-carrageenan could provide a better understanding of its functions in biological, medical and industrial applications. Chemical and physical analyses of carrageenan from seaweeds, Euchema cottonii L., were done to offer information on its properties and the effects of Co-60 γ-irradiation on its thermochemical characteristics. The structural and morphological characteris...

2017
Phuong Nguyen Tri Sandra Domenek Alain Guinault Cyrille Sollogoub Phuong Nguyen TRI Sandra DOMENEK Alain GUINAULT Cyrille SOLLOGOUB

The morphology and miscibility of commercial poly(lactide) (PLA)/poly(b-hydroxybutyrate) (PHB, from 5 to 20 wt %) blends prepared by melt extrusion method, were investigated using differential scanning calorimetry (DSC) and Fourier transform infrared spectroscopy (FTIR) observations. The results show that for all the studied blend contents, PLA/PHB blends are immiscible. The effects of PHB and ...

A. Hassanzadeh Hassanzadeh H.G. Mohammadi R Khodabakhsh

The variation of thermal and structural properties of 2-{[4-(2-hydroxybenzylideneamino) phenylimino]methyl}phenol (PAM)Schiff base were studied using differential scanning calorimetry (DSC) and powder X-ray diffraction techniques before and after fast neutron (1.050 and 1.740kGy), beta (11.01Gy) and gamma (453.0Gy) irradiations. Under fast neutron irradiation, the melting and decomposition enth...

2006
C. T. Carvalho A. B. Siqueira E. C. Rodrigues M. Ionashiro

Solid-state M-2-MeO-Bz compounds, where M stands for bivalent Mn, Co, Ni, Cu and Zn and 2-MeO-Bz is 2-methoxybenzoate, have been synthesized. Simultaneous thermogravimetry-differential thermal analysis (TG-DTA), thermogravimetry, derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy and complexometry were used to charac...

Journal: :Journal of visualized experiments : JoVE 2017
Ibrahim B Durowoju Kamaljit S Bhandal Jian Hu Bruce Carpick Marina Kirkitadze

Differential scanning calorimetry (DSC) is an analytical technique that measures the molar heat capacity of samples as a function of temperature. In the case of protein samples, DSC profiles provide information about thermal stability, and to some extent serves as a structural "fingerprint" that can be used to assess structural conformation. It is performed using a differential scanning calorim...

2007
I. Sinclair

The friction stir welding process has been used to join 13mm gauge 2024-T351 aluminium alloy plates together. A detailed microstructural study of the resulting weld was carried out using Differential Scanning Calorimetry (DSC), hardness testing, Scanning Electron Microscopy (SEM) and Electron Backscatter Diffraction (EBSD). DSC was used to explain the hardness results at a number of regions acr...

Journal: :Acta pharmaceutica 2007
Venkadari Rammohan Gupta Srinivas Mutalik Madhobhai M Patel Girish K Jani

Celecoxib spherical agglomerates were prepared with polyvinylpyrrolidone (PVP) using acetone, water and chloroform as solvent, non-solvent and bridging liquid, respectively. The agglomerates were characterized by differential scanning calorimetry (DSC), X-ray diffraction (XRD), IR spectroscopic studies and scanning electron microscopy (SEM). The IR spectroscopy and DSC results indicated the abs...

Acetylcholinesterase (AChE) enzyme which catalyses the hydrolysis of choline esters, such as acetylcholine, is very important in nerve function. Previous structural studies showed the possible amyloid fibril formation on the AChE. Therefore it is important to understand interaction of ligands to prevent the formation of  amyloid fibrils. The purpose of the present study was to  char...

2006

Many methods exist for the analysis and for the characterization of the phase transformations of the rapidly solidified alloys, which are also described in the literature [1 3]. frequently used methods are the scanning electron microscopy (sEM), transmission electron microscopy For the characterization of the phase transformations in the alloys during the heat treatment the various methods of t...

Journal: :Current medicinal chemistry 2005
G Bruylants J Wouters C Michaux

All biological phenomena depend on molecular recognition, which is either intermolecular like in ligand binding to a macromolecule or intramolecular like in protein folding. As a result, understanding the relationship between the structure of proteins and the energetics of their stability and binding with others (bio)molecules is a very interesting point in biochemistry and biotechnology. It is...

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